{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,6,18]],"date-time":"2026-06-18T00:43:27Z","timestamp":1781743407164,"version":"3.54.5"},"reference-count":24,"publisher":"Cambridge University Press (CUP)","issue":"3","license":[{"start":{"date-parts":[[2019,8,5]],"date-time":"2019-08-05T00:00:00Z","timestamp":1564963200000},"content-version":"unspecified","delay-in-days":4,"URL":"https:\/\/www.cambridge.org\/core\/terms"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Journal of Dairy Research"],"published-print":{"date-parts":[[2019,8]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>The experiments reported in this research paper aimed to investigate differences in the levels of chlorate (CHLO), perchlorate (PCHLO), trichloromethane (TCM) and iodine residues in bulk tank (BT) milk produced at different milk production periods, and to monitor those levels throughout a skim milk powder (SMP) production chain (BTs, collection tankers [CTs], whole milk silo [WMS] and skim milk silo [SMS]). Chlorate, PCHLO and iodine were measured in SMP, while TCM was measured in the milk cream. The CHLO, TCM and iodine levels in the mid-lactation milk stored in the WMS were lower than legislative and industrial specifications (0.0100 mg\/kg, 0.0015 mg\/kg and 150 \u00b5g\/l, respectively). However, in late-lactation, these levels were numerically higher than the mid-lactation levels and specifications. Trichloromethane accumulated in the cream portion after separation. Perchlorate was not detected in any of the samples. Regarding iodine, the levels in mid-lactation reconstituted SMP were higher than that required by manufacturers (100 \u00b5g\/l), indicating that the levels in milk should be lower than 142 \u00b5g\/l. The higher residue levels observed in late-lactation could be related to the low milk volume produced during that period and changes in sanitation practices, while changes in feed management could have affected iodine levels. This study could assist in controlling and setting limits for CHLO, TCM and iodine levels in milk, ensuring premium quality dairy products.<\/jats:p>","DOI":"10.1017\/s0022029919000578","type":"journal-article","created":{"date-parts":[[2019,8,5]],"date-time":"2019-08-05T08:03:03Z","timestamp":1564992183000},"page":"341-346","source":"Crossref","is-referenced-by-count":13,"title":["Monitoring residue concentrations in milk from farm and throughout a milk powder manufacturing process"],"prefix":"10.1017","volume":"86","author":[{"given":"Lizandra F.","family":"Paludetti","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Alan L.","family":"Kelly","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bernadette","family":"O'Brien","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"David","family":"Gleeson","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"56","published-online":{"date-parts":[[2019,8,5]]},"reference":[{"key":"S0022029919000578_ref6","doi-asserted-by":"publisher","DOI":"10.1007\/s00394-013-0597-4"},{"key":"S0022029919000578_ref17","doi-asserted-by":"publisher","DOI":"10.1017\/S0022029919000347"},{"key":"S0022029919000578_ref1","unstructured":"BS EN 15111:2007 (2007) Foodstuffs, Determination of trace elements, Determination of iodine by ICP-MS (inductively coupled plasma mass spectrometry). European Committee for standardization, Brussels, Belgium."},{"key":"S0022029919000578_ref16","first-page":"209","article-title":"Iodine concentrations in milk","volume":"52","author":"O'Brien","year":"2013","journal-title":"Irish Journal of Agricultural and Food Research"},{"key":"S0022029919000578_ref20","unstructured":"SAS (2016) Version 9.3, Cary, NC, USA: SAS Institute Inc."},{"key":"S0022029919000578_ref14","first-page":"129","article-title":"The effect of supplementary grass silage and standard concentrate on milk fat fatty acid composition and iodine value when cows are fed a whole rapeseed-based concentrate at pasture","volume":"49","author":"Magowan","year":"2010","journal-title":"Irish Journal of Agricultural and Food Research"},{"key":"S0022029919000578_ref8","unstructured":"Gleeson D (2016) Cleaning protocols for milking equipment to ensure low bacterial counts and minimum residues. Available at https:\/\/www.teagasc.ie\/media\/website\/animals\/dairy\/joint-programmes\/Arrabawn_conference2016.pdf. (Accessed 31 May 2018)."},{"key":"S0022029919000578_ref9","doi-asserted-by":"publisher","DOI":"10.1111\/1471-0307.12037"},{"key":"S0022029919000578_ref12","volume-title":"Chloroform","year":"1999"},{"key":"S0022029919000578_ref21","first-page":"686","article-title":"Model tests for the formation of TCM by chlorine containing cleaning and disinfection products","volume":"52","author":"Tiefel","year":"1997","journal-title":"Milchwissenschaft"},{"key":"S0022029919000578_ref15","first-page":"87","article-title":"Seasonal variation in the composition of Irish manufacturing and retail milks IV minerals and trace elements","volume":"38","author":"O'Brien","year":"1999","journal-title":"Irish Journal of Agricultural and Food Research"},{"key":"S0022029919000578_ref23","doi-asserted-by":"publisher","DOI":"10.1016\/j.scitotenv.2013.05.097"},{"key":"S0022029919000578_ref3","first-page":"1","article-title":"Regulation (EC) No 396\/2005 of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91\/414\/ECC","volume":"L70","year":"2005","journal-title":"Official Journal of the European Union"},{"key":"S0022029919000578_ref4","first-page":"1","article-title":"Opinion of the scientific panel on additives and products or substances used in animal feed on the request from the commission on the use of iodine in feeding stuffs","volume":"168","year":"2005","journal-title":"EFSA Journal"},{"key":"S0022029919000578_ref24","first-page":"1","article-title":"Risks for public related to the presence of chlorates in food. EFSA Panel on Contaminants in the Food Chain (CONTAM)","volume":"13","year":"2015","journal-title":"EFSA Journal"},{"key":"S0022029919000578_ref7","doi-asserted-by":"publisher","DOI":"10.1016\/j.scitotenv.2010.03.011"},{"key":"S0022029919000578_ref10","doi-asserted-by":"publisher","DOI":"10.1021\/es00015a014"},{"key":"S0022029919000578_ref11","volume-title":"Food Safety and Quality Assurance: Foods of Animal Origin","author":"Hubbert","year":"1996"},{"key":"S0022029919000578_ref13","doi-asserted-by":"publisher","DOI":"10.1038\/nrendo.2013.251"},{"key":"S0022029919000578_ref19","doi-asserted-by":"publisher","DOI":"10.1017\/S0022029913000113"},{"key":"S0022029919000578_ref22","unstructured":"US National Research Council (2001) Nutrient Requirements of Dairy Cattle. Washington, DC, USA: National Academy Press. Available at http:\/\/www.nap.edu\/openbook.php?isbn=0309069971. (Accessed 14 June 2018)."},{"key":"S0022029919000578_ref5","unstructured":"European Union Reference Laboratories for Residues of Pesticides \u2013 Single Residue Methods (EURL-SRM) (2015) Quick Method for the Analysis of numerous Highly Polar Pesticides in Foods of Plant Origin via LC-MS\/MS involving simultaneous extraction with methanol (QuPPe-Method). Available at http:\/\/www.crl-pesticides.eu\/library\/docs\/srm\/meth_QuPPe.pdf. (Accessed 22 February 2018)."},{"key":"S0022029919000578_ref18","first-page":"418","article-title":"Chloroform in milk and dairy products. Part A: analysis of chloroform using static headspace gas chromatography","volume":"95","author":"Resch","year":"1999","journal-title":"Deutsche Lebensmittel-Rundschau"},{"key":"S0022029919000578_ref2","doi-asserted-by":"publisher","DOI":"10.1007\/978-1-4899-1245-9"}],"container-title":["Journal of Dairy Research"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/www.cambridge.org\/core\/services\/aop-cambridge-core\/content\/view\/S0022029919000578","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2020,1,23]],"date-time":"2020-01-23T13:09:40Z","timestamp":1579784980000},"score":1,"resource":{"primary":{"URL":"https:\/\/www.cambridge.org\/core\/product\/identifier\/S0022029919000578\/type\/journal_article"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2019,8]]},"references-count":24,"journal-issue":{"issue":"3","published-print":{"date-parts":[[2019,8]]}},"alternative-id":["S0022029919000578"],"URL":"https:\/\/doi.org\/10.1017\/s0022029919000578","relation":{},"ISSN":["0022-0299","1469-7629"],"issn-type":[{"value":"0022-0299","type":"print"},{"value":"1469-7629","type":"electronic"}],"subject":[],"published":{"date-parts":[[2019,8]]}}}