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Herein, we determined 11 HALSs in paired breast milk and urine samples from nursing mothers in South China. At least one HALS was detected in 98.7% of breast milk samples and 98.7% of urine samples, with \u2211HALS concentration ranges of &amp;lt; MDL-19.9 ng\/mL (median: 2.20 ng\/mL) and &amp;lt; MDL-23.0 ng\/mL (median: 1.29 ng\/mL), respectively. HALS compositions differed between breast milk and urine samples and 4-hydroxy-1-(2-hydroxyethyl)-2,2,6,6-tetramethylpiperidine (HA 201) was the dominant compound. Most intercompound correlations were weak, suggesting compound-specific sources and toxicokinetic behaviors. In paired-sample regression analyses, breast milk concentrations of HA 201 and methyl 1,2,2,6,6-pentamethyl-4-piperidyl sebacate (HS 508) showed weak but statistically significant positive associations with corresponding urinary concentrations. In exploratory analyses, recent home renovation, frequent plastic-packaged convenience food consumption, and greater personal care product use were associated with higher HALS levels. Under high exposure scenario, breastfeeding-mediated intakes of bis(1,2,2,6,6-pentamethyl-4-piperidyl) butyl(3,5-ditert-butyl-4-hydroxybenzyl) malonate (Tinuvin 144) in infants younger than 3 months exceeded the predicted reference dose, indicating a screening-level risk signal. This biomonitoring evidence of HALSs in human biological samples highlights the need for expanded exposure and toxicity studies.<\/jats:p>","DOI":"10.1021\/acs.est.6c08937","type":"journal-article","created":{"date-parts":[[2026,8,19]],"date-time":"2026-08-19T15:01:23Z","timestamp":1787151683000},"page":"23892-23900","source":"Crossref","is-referenced-by-count":0,"title":["Occurrence and Human\nExposure Assessment of Emerging\nHindered Amine Light Stabilizers in Paired Breast Milk and Urine from\nNursing Mothers in South China"],"prefix":"10.1021","volume":"60","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-4400-6493","authenticated-orcid":true,"given":"Xiang","family":"Ge","sequence":"first","affiliation":[{"name":"Guizhou University , , ,","place":["Guiyang, China, 550025"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4815-3431","authenticated-orcid":true,"given":"Lixi","family":"Zeng","sequence":"additional","affiliation":[{"name":"Guizhou University , , ,","place":["Guiyang, China, 550025"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Aizhen","family":"Su","sequence":"additional","affiliation":[{"name":"Jinan University , , ,","place":["Guangzhou, China, 511443"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xuejia","family":"Yao","sequence":"additional","affiliation":[{"name":"Jinan University , , ,","place":["Guangzhou, China, 511443"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jingwei","family":"Zhao","sequence":"additional","affiliation":[{"name":"Jinan University , , ,","place":["Guangzhou, China, 511443"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jiali","family":"Ge","sequence":"additional","affiliation":[{"name":"Jinan University , , ,","place":["Guangzhou, China, 511443"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4977-2437","authenticated-orcid":true,"given":"Bibai","family":"Du","sequence":"additional","affiliation":[{"name":"Jinan University , , ,","place":["Guangzhou, China, 511443"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,19]]},"reference":[{"key":"2026090307150572800_cit1","doi-asserted-by":"publisher","first-page":"179","DOI":"10.1016\/j.jhazmat.2017.10.014","article-title":"An overview of chemical additives present in plastics:\nMigration, release, fate and environmental impact during their use,\ndisposal and recycling","volume":"344","author":"Hahladakis","year":"2018","journal-title":"J. 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Global\nHindered Amine Light Stabilizers (HALS) Market Research Report (Status\nand Outlook)2022https:\/\/www.asdreports.com\/market-research-report-605415\/global-hindered-amine-light-stabilizers-hals-market-research-report-status. (accessed June 3, 2026)."},{"issue":"2","key":"2026090307150572800_cit8","doi-asserted-by":"publisher","first-page":"1349","DOI":"10.1021\/acs.est.3c08884","article-title":"First Evidence\nof Hindered Amine Light Stabilizers As Abundant, Ubiquitous, Emerging\nPollutants in Dust and Air Particles: A New Concern for Human Health","volume":"58","author":"Deng","year":"2024","journal-title":"Environ. Sci. Technol."},{"issue":"12","key":"2026090307150572800_cit9","doi-asserted-by":"publisher","first-page":"1656","DOI":"10.1021\/acs.estlett.5c00875","article-title":"Discovery of Hindered\nAmine Light Stabilizers in Dust from Automotive Repair Shops in China","volume":"12","author":"Fang","year":"2025","journal-title":"Environ. Sci. Technol. 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Technol."},{"key":"2026090307150572800_cit22","doi-asserted-by":"publisher","DOI":"10.1093\/clinchem\/hvaf086.704","article-title":"B-317 Detection\nof bis(2,2,6,6-tetramethyl-4-piperidyl)\nsebacate (BTMPS) throughout the United States in healthcare patient\nurine samples","volume":"71","author":"David","year":"2025","journal-title":"Clin. Chem."},{"issue":"3","key":"2026090307150572800_cit23","doi-asserted-by":"publisher","first-page":"206","DOI":"10.1021\/acs.estlett.0c00104","article-title":"Co-occurrence of and Infant Exposure\nto Multiple Common and Unusual\nPhenolic Antioxidants in Human Breast Milk","volume":"7","author":"Zhang","year":"2020","journal-title":"Environ. Sci. Technol. 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