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In this research, X-ray absorption near-edge structure analysis was conducted to quantify the transformation of Fe and P species in the sludge of different aging periods and in the subsequent acidogenic cofermentation for P recovery. P was readily removed from wastewater by Fe-facilitated coprecipitation and adsorption and could be extracted and recovered from sludge via acidogenic cofermentation and microbial iron reduction with food waste. The fresh Fe-based sludge mainly contained fresh ferrihydrite and amorphous FePO4 with sufficient accessible surface area, which was favorable for Fe\u2013P mobilization and dissolution via microbial reaction. Ferric iron dosed into wastewater underwent rapid hydrolysis, clustering, aggregation, and slow crystallization to form hydrous iron oxides (HFO) with various complicated structures. With the aging of sludge in bioreactors, the HFO densified into phases with much reduced surface area and reactivity (e.g., goethite), which greatly increased the difficulty of P release and recovery. Thus, aging of P-containing sludge should be minimized in wastewater treatment systems for the purpose of P recovery.<\/jats:p>","DOI":"10.1021\/acs.est.9b07138","type":"journal-article","created":{"date-parts":[[2020,3,13]],"date-time":"2020-03-13T15:32:32Z","timestamp":1584113552000},"page":"4641-4650","source":"Crossref","is-referenced-by-count":50,"title":["Transformation\nof Fe\u2013P Complexes in Bioreactors\nand P Recovery from Sludge: Investigation by XANES Spectroscopy"],"prefix":"10.1021","volume":"54","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-7649-0016","authenticated-orcid":true,"given":"Ruo-hong","family":"Li","sequence":"first","affiliation":[{"name":"Tsinghua University , , ,","place":["Shenzhen, China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jin-li","family":"Cui","sequence":"additional","affiliation":[{"name":"The Hong Kong Polytechnic University , , , ,","place":["Hung Hom, Kowloon, Hong Kong, China"]},{"name":"Guangzhou University , , ,","place":["Guangzhou, China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jia-hui","family":"Hu","sequence":"additional","affiliation":[{"name":"Tsinghua University , , ,","place":["Shenzhen, China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wei-jun","family":"Wang","sequence":"additional","affiliation":[{"name":"Tsinghua University , , ,","place":["Shenzhen, China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7161-0477","authenticated-orcid":true,"given":"Bing","family":"Li","sequence":"additional","affiliation":[{"name":"Tsinghua University , , ,","place":["Shenzhen, China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4044-2888","authenticated-orcid":true,"given":"Xiang-dong","family":"Li","sequence":"additional","affiliation":[{"name":"The Hong Kong Polytechnic University , , , ,","place":["Hung Hom, Kowloon, Hong Kong, China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1910-2464","authenticated-orcid":true,"given":"Xiao-yan","family":"Li","sequence":"additional","affiliation":[{"name":"Tsinghua University , , ,","place":["Shenzhen, China"]},{"name":"The University of Hong Kong , , , ,","place":["Pokfulam, Hong Kong, China"]},{"name":"Tsinghua University , , ,","place":["Shenzhen, China"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2020,3,13]]},"reference":[{"issue":"2","key":"2026081715242319900_cit1","doi-asserted-by":"publisher","first-page":"292","DOI":"10.1016\/j.gloenvcha.2008.10.009","article-title":"The story of phosphorus: global food\nsecurity and food for thought","volume":"19","author":"Cordell","year":"2009","journal-title":"Global Environ.\nChange"},{"key":"2026081715242319900_cit2","volume-title":"Environmental quality\nstandards for surface water (GB3838-2002), Ministry of Ecology and\nEnviornment, PR China","author":"MEE","year":"2003"},{"issue":"6","key":"2026081715242319900_cit3","doi-asserted-by":"publisher","first-page":"1298","DOI":"10.2166\/wst.2011.145","article-title":"Enhanced nutrient removal\nMBR system with chemical addition for low effluent TP","volume":"64","author":"Liu","year":"2011","journal-title":"Water Sci. 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