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These materials demonstrate three distinct functions: sensing low-concentration formic acid vapor, lysosome imaging in living cells, and photocatalytic wastewater purification. Specifically, the Ln-PTTA-MOFs feature a layered network structure formed by the alternating linkage of H4PTTA ligands and LnO8. Among them, Eu-PTTA-MOF exhibits a highly selective and visually perceptible optical response to low-concentration formic acid vapor, achieving a detection limit as low as 3.1 ppm. Notably, the highly luminescent, nanoscale Eu-PTTA-MOF enables high-resolution optical imaging of various cancer cells. Co-localization analysis reveals that Eu-PTTA-MOF nanosheets efficiently localize within the lysosomes of living cells, with a colocalization coefficient exceeding 0.93. By leveraging the heavy-atom effect of the lanthanide ions within the SBUs and the high molar extinction coefficient of the organic ligands, the Ln-PTTA-MOFs can generate a \u201creactive oxygen species storm\u201d even under low-power light irradiation. Consequently, they exhibit excellent photocatalytic degradation performance against organic dyes and antibiotics. This work paves a new way for the design of multifunctional lanthanide metal\u2013organic frameworks that integrate luminescent sensing, bioimaging, and photocatalytic degradation capabilities.<\/jats:p>","DOI":"10.1021\/acs.inorgchem.6c02834","type":"journal-article","created":{"date-parts":[[2026,7,20]],"date-time":"2026-07-20T13:22:16Z","timestamp":1784553736000},"page":"17788-17799","source":"Crossref","is-referenced-by-count":0,"title":["Brightly Luminescent AIEgens-Based Layered Lanthanide\nOrganic Frameworks: Photoresponsive Formic Acid Vapor Sensing, Intracellular\nLysosome Imaging, and Photocatalytic Wastewater Treatment"],"prefix":"10.1021","volume":"65","author":[{"given":"Chang-Jia","family":"Wu","sequence":"first","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"De-Xin","family":"Chen","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fan","family":"Yang","sequence":"additional","affiliation":[{"name":"Guangxi Normal University , , ,","place":["Guilin, P. R. China, 541004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ru-Yan","family":"Li","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yun-Lan","family":"Li","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. 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