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In this study, two structurally robust and water-stable Ln-MOFs (Eu-MOF and Gd-MOF) were synthesized by assembling the ligand 4,4\u2032-(anthracene-9,10-diyl)dibenzoic acid (H2ADBA) with Eu2O17 and Gd2O16 secondary building units, respectively. The deprotonated ADBA2\u2013 ligands adopt a Z+-shaped arrangement with a dihedral angle of 52.71\u00b0 between adjacent anthracene rings; this configuration suppresses interligand \u03c0\u2013\u03c0 stacking and reduces radiative transition losses, thereby significantly enhancing ROS generation efficiency. Fluorescence probe and electron paramagnetic resonance (EPR) analyses confirmed that both Ln-MOFs could generate Type I and Type II ROS under irradiation from a low-power (60 mW\/cm2) xenon lamp. These Ln-MOFs achieved near-complete degradation of 10 mg\/L Rhodamine B and Methylene Blue within 30 and 90 min, respectively; furthermore, they demonstrated excellent performance in antibiotic degradation and antibacterial activity against Escherichia coli and Staphylococcus aureus. This work offers a strategy for the rational design of high-performance Ln-MOF photosensitizers for wastewater purification and sterilization.<\/jats:p>","DOI":"10.1021\/acs.inorgchem.6c03076","type":"journal-article","created":{"date-parts":[[2026,8,14]],"date-time":"2026-08-14T14:02:11Z","timestamp":1786716131000},"page":"19998-20010","source":"Crossref","is-referenced-by-count":1,"title":["Regulating\nthe Arrangement of Planar Ligands in Lanthanide\nMetal\u2013Organic Framework Photosensitizers to Induce a Photocatalytic\nReactive Oxygen Species Storm for Sewage Purification and Photodynamic\nSterilization"],"prefix":"10.1021","volume":"65","author":[{"given":"Fan","family":"Yang","sequence":"first","affiliation":[{"name":"Guangxi Normal University , , ,","place":["Guilin, P. R. China, 541004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yun-Lan","family":"Li","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. 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China, 541004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1968-4855","authenticated-orcid":true,"given":"Zhong-Hong","family":"Zhu","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,14]]},"reference":[{"issue":"19","key":"2026090222513326300_cit1","doi-asserted-by":"publisher","first-page":"12466","DOI":"10.1021\/acs.chemrev.6b00346","article-title":"Structures of Metal-Organic\nFrameworks with Rod Secondary Building Units","volume":"116","author":"Schoedel","year":"2016","journal-title":"Chem. 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