{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,3]],"date-time":"2026-09-03T03:15:39Z","timestamp":1788405339593,"version":"build-2803163510"},"reference-count":51,"publisher":"American Chemical Society (ACS)","issue":"34","license":[{"start":{"date-parts":[[2026,8,18]],"date-time":"2026-08-18T00:00:00Z","timestamp":1787011200000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100004410","name":"T?rkiye Bilimsel ve Teknolojik Arastirma Kurumu","doi-asserted-by":"publisher","award":["222Z040"],"award-info":[{"award-number":["222Z040"]}],"id":[{"id":"10.13039\/501100004410","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,8,31]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>Manganese is an earth-abundant, low-cost transition metal with considerable potential for sustainable electrocatalysis; however, its poor stability under oxidative alkaline conditions remains a major challenge. Herein, we report the fabrication of Ni(II)- and Co(II)-substituted olivine lithium manganese phosphate electrodes, LiMn1\u2013xMxPO4 (M = Ni, Co; x = 0.05, 0.10, and 0.25), through an alcohol-mediated synthesis approach and investigate the effects of solvent and secondary metal incorporation on their structural evolution and alkaline oxygen evolution reaction (OER) performance. The precursor solutions exhibit markedly different precipitation behaviors depending on the solvent. Rapid precipitation of crystalline MnPO4\u00b7H2O occurs in ethanol and 1-butanol, whereas precipitation is slower and less extensive in methanol. Increasing Ni(II) concentration suppresses precipitation more effectively than Co(II), improving the stabilization of Mn(II) in solution. Upon calcination, ethanol- and 1-butanol-derived precursors yield predominantly mesoporous olivine LiMn1\u2013xMxPO4 with minor Mn2P2O7 impurities, whereas methanol-derived solutions and supernatants produce phase-pure olivine LiMn1\u2013xMxPO4. Electrochemical studies in 1 M KOH reveal rapid reconstruction of all phosphate electrodes into mixed-metal hydroxides, identifying these hydroxides as the active OER species. Secondary metal incorporation substantially enhances electrode stability by suppressing manganese degradation and promoting stable mixed (Mn,M)(OH)2 active phases.<\/jats:p>","DOI":"10.1021\/acs.inorgchem.6c03469","type":"journal-article","created":{"date-parts":[[2026,8,18]],"date-time":"2026-08-18T22:02:07Z","timestamp":1787090527000},"page":"20104-20121","source":"Crossref","is-referenced-by-count":0,"title":["Mesoporous LiMn1\u2013xMxPO4 (M\n= Ni, Co) Precatalysts by Alcohol-Mediated Self-Assembly:\nHydroxide Reconstruction and Suppression of Manganese Degradation\nfor Stable Alkaline Oxygen Evolution"],"prefix":"10.1021","volume":"65","author":[{"given":"Arda","family":"Altan","sequence":"first","affiliation":[{"name":"Bilkent University , , ,","place":["Ankara, Tu\u0308rkiye, 06800"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Irmak Karakaya","family":"Durukan","sequence":"additional","affiliation":[{"name":"Bilkent University , , ,","place":["Ankara, Tu\u0308rkiye, 06800"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1129-3246","authenticated-orcid":true,"given":"O\u0308mer","family":"Dag","sequence":"additional","affiliation":[{"name":"Bilkent University , , ,","place":["Ankara, Tu\u0308rkiye, 06800"]},{"name":"Bilkent University , , ,","place":["Ankara, Tu\u0308rkiye, 06800"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,18]]},"reference":[{"issue":"6","key":"2026090222513498000_cit1","doi-asserted-by":"publisher","first-page":"16023","DOI":"10.1038\/natrevmats.2016.23","article-title":"Mesoporous\nMaterials for Energy Conversion and Storage\nDevices","volume":"1","author":"Li","year":"2016","journal-title":"Nat. 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Technol."},{"key":"2026090222513498000_cit30","doi-asserted-by":"publisher","first-page":"842","DOI":"10.1016\/j.ensm.2021.07.017","article-title":"Recent Advances\nof Metal Phosphates-Based Electrodes for High-Performance Metal Ion\nBatteries","volume":"41","author":"Cheng","year":"2021","journal-title":"Energy Storage Mater."},{"key":"2026090222513498000_cit31","doi-asserted-by":"publisher","first-page":"15006","DOI":"10.1039\/C9TA04274A","article-title":"A Review on\nPyrophosphate Framework\nCathode Materials for Sodium-Ion Batteries","volume":"7","author":"Niu","year":"2019","journal-title":"J. Mater. Chem. A"},{"issue":"10","key":"2026090222513498000_cit32","doi-asserted-by":"publisher","DOI":"10.1002\/aenm.202505808","article-title":"A Review of Revealing the Impact of Transition Metals\nin Polyanionic Cathode Material Na4M3(PO4)2P2O7: Kinetic, Mechanisms\nand Optimization Strategies","volume":"16","author":"Yan","year":"2026","journal-title":"Adv. Energy Mater."},{"key":"2026090222513498000_cit33","doi-asserted-by":"publisher","first-page":"1544","DOI":"10.1002\/cplu.201900435","article-title":"Lyotropic Liquid Crystalline Mesophases\nMade of Salt\u2013Acid\u2013Surfactant Systems for the Synthesis\nof Novel Mesoporous Lithium Metal Phosphates","volume":"84","author":"Uzunok","year":"2019","journal-title":"ChemPlusChem"},{"key":"2026090222513498000_cit34","doi-asserted-by":"publisher","first-page":"22384","DOI":"10.1039\/D3TA05578G","article-title":"Fabrication of Mesoporous Nickel\nPyrophosphate Electrodes and Their Transformation to Nickel Hydroxide\nwith Decent Capacitance in Alkaline Media","volume":"11","author":"Ulu","year":"2023","journal-title":"J.\nMater. Chem. A"},{"key":"2026090222513498000_cit35","doi-asserted-by":"publisher","first-page":"16994","DOI":"10.1021\/acs.inorgchem.3c02808","article-title":"Nanoarchitectonics of Mesoporous\nM2P2O7 (M = Mn(II), Co(II), and Ni(II))\nand M2-xCoxP2O7 and Transformation to Their Metal Hydroxides with Decent Charge\nCapacity in Alkaline Media","volume":"62","author":"Ulu","year":"2023","journal-title":"Inorg. Chem."},{"key":"2026090222513498000_cit36","doi-asserted-by":"publisher","first-page":"6645","DOI":"10.1021\/acsaem.6c01082","article-title":"Alcohol-Mediated\nSelf-Assembling Nanoarchitectonics of Mesoporous LiMPO4 and M2P2O7 (M = Mn, Co, and Ni)\nfor Alkaline OER via Metal Hydroxide Transformation","volume":"9","author":"Altan","year":"2026","journal-title":"ACS Appl. Energy Mater."},{"key":"2026090222513498000_cit37","doi-asserted-by":"publisher","first-page":"938","DOI":"10.1021\/acs.inorgchem.5c05373","article-title":"Scalable Solvent-Mediated\nNanoarchitectonics of High-Surface-Area Mesoporous Ni2P2O7 for Enhanced Electrochemical Performance in\nAlkaline Media","volume":"65","author":"Ceran","year":"2026","journal-title":"Inorg. 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Mater."},{"key":"2026090222513498000_cit40","doi-asserted-by":"publisher","first-page":"103729","DOI":"10.1016\/j.est.2021.103729","article-title":"Issues and Opportunities\nof Manganese-Based Materials for Enhanced Zn-Ion Storage Performances","volume":"45","author":"Zhang","year":"2022","journal-title":"J. Energy Storage"},{"key":"2026090222513498000_cit41","doi-asserted-by":"publisher","first-page":"140294","DOI":"10.1016\/j.electacta.2022.140294","article-title":"Characterization,\nand Degradation Study of Mn-Based Phosphate Frameworks (Na2MnTi(PO4)2, Na2MnPO4CO2, Na4Mn2(PO4)2P2O7) as Aqueous Na-Ion Battery Positive Electrodes","volume":"417","author":"Tediashvili","year":"2022","journal-title":"Electrochim. Acta"},{"key":"2026090222513498000_cit42","doi-asserted-by":"publisher","first-page":"1853","DOI":"10.1002\/anie.201107394","article-title":"Double-Structured\nLiMn0.85Fe0.15PO4 Coordinated with\nLiFePO4 for Rechargeable\nLithium Batteries","volume":"51","author":"Oh","year":"2012","journal-title":"Angew. Chem., Int. Ed."},{"key":"2026090222513498000_cit43","doi-asserted-by":"publisher","first-page":"6359","DOI":"10.1039\/D3TA07973B","article-title":"Manganese\nOxide-Based Mesoporous Thin-Film Electrodes:\nManganese Disproportionation Reaction in Alkaline Media","volume":"12","author":"Durukan","year":"2024","journal-title":"J. Mater. Chem. A"},{"issue":"13","key":"2026090222513498000_cit44","doi-asserted-by":"publisher","DOI":"10.1002\/celc.202200482","article-title":"Stabilization of a Mn\u2013Co Oxide\nDuring Oxygen Evolution in Alkaline Media","volume":"9","author":"Villalobos","year":"2022","journal-title":"ChemElectroChem"},{"key":"2026090222513498000_cit45","doi-asserted-by":"publisher","first-page":"2487","DOI":"10.1016\/S0013-4686(01)00449-2","article-title":"Anodic Behaviour\nof Manganese in Alkaline Medium","volume":"46","author":"Messaoudi","year":"2001","journal-title":"Electrochim.\nActa"},{"key":"2026090222513498000_cit46","doi-asserted-by":"publisher","first-page":"11007","DOI":"10.1021\/nn505199q","article-title":"Highly\nProton Conductive Phosphoric Acid\u2013Nonionic Surfactant Lyotropic\nLiquid Crystalline Mesophases and Application in Graphene Optical\nModulators","volume":"8","author":"Tunkara","year":"2014","journal-title":"ACS Nano"},{"issue":"1\u20132","key":"2026090222513498000_cit47","doi-asserted-by":"publisher","first-page":"78","DOI":"10.1016\/j.jallcom.2006.12.064","article-title":"Nanocrystalline\nSerrabrancaite (MnPO4\u00b7H2O) Prepared by\na Simple Precipitation Route at Low Temperature","volume":"454","author":"Boonchom","year":"2008","journal-title":"J. Alloys Comp."},{"key":"2026090222513498000_cit48","doi-asserted-by":"publisher","first-page":"1334","DOI":"10.1021\/ic00332a009","article-title":"Characterization of Manganese(III)\nOrthophosphate Hydrate","volume":"29","author":"Aranda","year":"1990","journal-title":"Inorg. Chem."},{"key":"2026090222513498000_cit49","doi-asserted-by":"publisher","first-page":"1051","DOI":"10.1515\/pac-2014-1117","article-title":"Physisorption of Gases, with Special\nReference to the Evaluation of Surface Area and Pore Size Distribution\n(IUPAC Technical Report)","volume":"87","author":"Thommes","year":"2015","journal-title":"Pure Appl. Chem."},{"key":"2026090222513498000_cit50","doi-asserted-by":"publisher","first-page":"47","DOI":"10.1016\/j.susc.2018.04.022","article-title":"Oxidation of MnO(100)\nand NaMnO2 Formation:\nCharacterization of Mn2+ and Mn3+ Surfaces via\nXPS and Water TPD","volume":"675","author":"Feng","year":"2018","journal-title":"Surf. Sci."},{"key":"2026090222513498000_cit51","doi-asserted-by":"publisher","first-page":"3057","DOI":"10.1021\/acsaem.0c02710","article-title":"Efficient\nOxygen Evolution Electrocatalysis on CaFe2O4 and its Reaction Mechanism","volume":"4","author":"Sugawara","year":"2021","journal-title":"ACS Appl. Energy\nMater."}],"container-title":["Inorganic Chemistry"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/pubs.acs.org\/doi\/pdf\/10.1021\/acs.inorgchem.6c03469","content-type":"application\/pdf","content-version":"vor","intended-application":"unspecified"},{"URL":"https:\/\/pubs.acs.org\/inocaj\/article-pdf\/65\/34\/20104\/66855562\/acs.inorgchem.6c03469.pdf","content-type":"application\/pdf","content-version":"vor","intended-application":"syndication"},{"URL":"https:\/\/pubs.acs.org\/inocaj\/article-pdf\/65\/34\/20104\/66855562\/acs.inorgchem.6c03469.pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2026,9,3]],"date-time":"2026-09-03T02:53:37Z","timestamp":1788404017000},"score":1,"resource":{"primary":{"URL":"https:\/\/pubs.acs.org\/inocaj\/article\/65\/34\/20104\/5275798\/Mesoporous-LiMn1-xMxPO4-M-Ni-Co-Precatalysts-by"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2026,8,18]]},"references-count":51,"journal-issue":{"issue":"34","published-online":{"date-parts":[[2026,8,18]]},"published-print":{"date-parts":[[2026,8,31]]}},"URL":"https:\/\/doi.org\/10.1021\/acs.inorgchem.6c03469","relation":{},"ISSN":["0020-1669","1520-510X"],"issn-type":[{"value":"0020-1669","type":"print"},{"value":"1520-510X","type":"electronic"}],"subject":[],"published":{"date-parts":[[2026,8,18]]}}}