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However, achieving selective C\u2013C bond cleavage and subsequent C\u2013N bond formation with compatible catalysts remains challenging. This work reports an inexpensive CuI-catalyzed oxidative amidation of lignin \u03b2-O-4 moieties, primary alcohols, and secondary alcohols with aromatic amines under an oxygen atmosphere, yielding diverse functionalized aromatic amides in moderate to high yields, up to 86%. Mechanistic investigations suggest a reaction pathway involving the selective oxidation of benzylic alcohol, followed by the key C\u2013C bond cleavage, C\u2013N bond formation, and final dehydrogenative oxidation. Furthermore, bioassay results showed that most of the synthesized amide derivatives exhibit superior antifungal efficacy against six plant-pathogenic fungi compared with the commercial fungicides ethylicin and azoxystrobin at 100 \u03bcg\/mL. Here, we present a practical protocol for synthesizing aromatic amides that effectively links lignin valorization to crop-protection chemicals.<\/jats:p>","DOI":"10.1021\/acs.jafc.6c01445","type":"journal-article","created":{"date-parts":[[2026,7,16]],"date-time":"2026-07-16T13:32:26Z","timestamp":1784208746000},"page":"23599-23609","source":"Crossref","is-referenced-by-count":0,"title":["Sustainable Production\nof Amide-Based Fungicidal Agents\nfrom Lignin \u03b2-O-4 Motifs and Alcohols"],"prefix":"10.1021","volume":"74","author":[{"given":"Lu","family":"Chen","sequence":"first","affiliation":[{"name":"Fujian Agriculture and Forestry University , , ,","place":["Fuzhou, China, 350002"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiaoli","family":"Lou","sequence":"additional","affiliation":[{"name":"Fujian Agriculture and Forestry University , , , ,","place":["Fuzhou, Fujian, China, 350002"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yaqiu","family":"Zhao","sequence":"additional","affiliation":[{"name":"China Academy of Chinese Medical Sciences , , ,","place":["Beijing, China, 100700"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Kejing","family":"Xie","sequence":"additional","affiliation":[{"name":"Chongqing University of Arts and Sciences , , ,","place":["Chongqing, China, 402160"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lili","family":"Shao","sequence":"additional","affiliation":[{"name":"Fujian Agriculture and Forestry University , , ,","place":["Fuzhou, China, 350002"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jiayi","family":"Wu","sequence":"additional","affiliation":[{"name":"Fujian Agriculture and Forestry University , , ,","place":["Fuzhou, China, 350002"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yiyi","family":"Huang","sequence":"additional","affiliation":[{"name":"Fujian Agriculture and Forestry University , , ,","place":["Fuzhou, China, 350002"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yijia","family":"Hou","sequence":"additional","affiliation":[{"name":"Fujian Agriculture and Forestry University , , ,","place":["Fuzhou, China, 350002"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Li","family":"Shuai","sequence":"additional","affiliation":[{"name":"Fujian Agriculture and Forestry University , , ,","place":["Fuzhou, China, 350002"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,7,16]]},"reference":[{"key":"2026080510100252400_cit1","doi-asserted-by":"publisher","first-page":"471","DOI":"10.1038\/nature10702","article-title":"Rethinking amide bond synthesis","volume":"480","author":"Pattabiraman","year":"2011","journal-title":"Nature"},{"key":"2026080510100252400_cit2","doi-asserted-by":"publisher","first-page":"98","DOI":"10.1038\/s41929-018-0215-1","article-title":"Challenges\nand outlook for catalytic direct amidation reactions","volume":"2","author":"Wang","year":"2019","journal-title":"Nat. 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Soc.\nRev."},{"key":"2026080510100252400_cit6","doi-asserted-by":"publisher","first-page":"2714","DOI":"10.1039\/C3CS60345H","article-title":"Catalytic\namide formation from non-activated carboxylic acids and amines","volume":"43","author":"Lundberg","year":"2014","journal-title":"Chem. Soc. Rev."},{"key":"2026080510100252400_cit7","doi-asserted-by":"publisher","first-page":"606","DOI":"10.1039\/B701677H","article-title":"Amide bond formation: beyond the myth of coupling reagents","volume":"38","author":"Valeur","year":"2009","journal-title":"Chem. Soc. Rev."},{"key":"2026080510100252400_cit8","doi-asserted-by":"crossref","first-page":"2544","DOI":"10.1002\/cber.188401702178","article-title":"The oxidation\nof piperidines","volume":"21","author":"Schotten","year":"1884","journal-title":"Chem. Ber."},{"key":"2026080510100252400_cit9","doi-asserted-by":"publisher","first-page":"3218","DOI":"10.1002\/cber.188601902348","article-title":"A method for\nthe synthesis of benzoyl esters","volume":"19","author":"Baumann","year":"1886","journal-title":"Chem. Ber."},{"key":"2026080510100252400_cit10","doi-asserted-by":"publisher","first-page":"277","DOI":"10.1002\/9780470771082.ch6","article-title":"Substitution at\nan amino nitrogen","author":"Challis","year":"1968","journal-title":"Chem. Amino Group"},{"key":"2026080510100252400_cit11","doi-asserted-by":"publisher","first-page":"1254","DOI":"10.1002\/ejoc.200300620","article-title":"Chemoselective acylation\nof amines in aqueous media","volume":"2004","author":"Naik","year":"2004","journal-title":"Eur. J. Org. 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