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We introduce micelle\u2013solvent synergistic extraction (MSSE), a cleanup-free sample pretreatment platform that utilizes surfactant micelles to encapsulate target molecules from complex matrices, followed by solvent-induced release, thereby eliminating centrifugation, filtration, and sorbent-based cleanup. MSSE enabled rapid extraction of chemically distinct analytes, including a fungicide, herbicide, and fluorescent dye, from tobacco leaves and demonstrated its feasibility in soil and groundwater, requiring \u22645 min of sample preparation and only 0.9 mL of the extraction mixture. Compared with a representative literature-reported QuEChERS sample-preparation protocol, MSSE reduced solvent consumption by 91.0% and processing time by at least 88.4%. When integrated with portable surface-enhanced Raman spectroscopy, MSSE enabled rapid detection of the investigated analytes within the experimentally validated concentration ranges. These results establish MSSE as a rapid sample pretreatment strategy with potential for point-of-need analysis across agricultural and environmental applications.<\/jats:p>","DOI":"10.1021\/acs.jafc.6c08065","type":"journal-article","created":{"date-parts":[[2026,10,8]],"date-time":"2026-10-08T10:01:49Z","timestamp":1791453709000},"page":"32720-32733","source":"Crossref","is-referenced-by-count":0,"title":["Micelle\u2013Solvent\nSynergistic Extraction for\nRapid, Cleanup-Free SERS Analysis of Carbendazim in Tobacco Leaves"],"prefix":"10.1021","volume":"74","author":[{"ORCID":"https:\/\/orcid.org\/0009-0005-8397-9844","authenticated-orcid":true,"given":"Junaid","family":"Younus","sequence":"first","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 610054"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0004-8340-1025","authenticated-orcid":true,"given":"Qi","family":"Wang","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 610054"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shan","family":"Gao","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 610054"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"RuiQi","family":"Xie","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 610054"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiaowei","family":"Guo","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 610054"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xue","family":"Yang","sequence":"additional","affiliation":[{"name":"China National Tobacco Corporation Sichuan Company , ,","place":["Chengdu, China, 610041"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jimin","family":"Shao","sequence":"additional","affiliation":[{"name":"China National Tobacco Corporation Sichuan Provincial Tobacco Quality Supervision and Inspection Station , ,","place":["Chengdu, China, 610041"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,10,8]]},"reference":[{"key":"2026102109074180500_cit1","doi-asserted-by":"publisher","first-page":"137096","DOI":"10.1016\/j.jclepro.2023.137096","article-title":"Industry 4.0 Technologies in Agri-Food\nSector and Their Integration in the Global Value Chain: A Review","volume":"408","author":"Senturk","year":"2023","journal-title":"J. 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