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Conventional methods rely on harsh conditions, causing severe degradation of cellulose and hemicellulose and lignin condensation, while milder conditions compromise fractionation efficiency. To balance native structure preservation and fractionation efficiency, a biphasic system composed of lithium bromide molten salt hydrate (MSH) and n-butanol was developed. At 110 \u00b0C for 1 h, cellulose and hemicellulose were selectively hydrolyzed into oligosaccharides in the MSH phase with yields of 81.4% and 88.1%, respectively. The isolated lignin retained 96.1% of \u03b2-O-4 ether bonds (38.5\/100 C9 units), and its catalytic hydrogenolysis delivered a monophenol yield of 82.1% to the theoretical value. The light-colored lignin (\u0394E = 31.28) achieved SPF 28.2 as a sole sunscreen active ingredient, demonstrating commercial potential. This biphasic system enables highly selective fractionation of lignocellulosic components with limited condensation, yielding key feedstocks for bioenergy and biorefinery, including oligosaccharides and native structure-preserved lignin.<\/jats:p>","DOI":"10.1021\/acs.jafc.6c08285","type":"journal-article","created":{"date-parts":[[2026,7,27]],"date-time":"2026-07-27T08:17:42Z","timestamp":1785140262000},"page":"23451-23460","source":"Crossref","is-referenced-by-count":0,"title":["Selective Fractionation\nof Larch into Oligosaccharides\nand Less-Condensed Lignin in a Novel Molten Salt\/\n                    <i>n<\/i>\n                    -Butanol System"],"prefix":"10.1021","volume":"74","author":[{"given":"Yuetong","family":"Huang","sequence":"first","affiliation":[{"name":"Guangdong University of Technology , , ,","place":["Guangzhou, China, 510006"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xinyan","family":"Zhang","sequence":"additional","affiliation":[{"name":"Guangdong University of Technology , , ,","place":["Guangzhou, China, 510006"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6860-5028","authenticated-orcid":true,"given":"Qiyu","family":"Liu","sequence":"additional","affiliation":[{"name":"Guangdong University of Technology , , ,","place":["Guangzhou, China, 510006"]},{"name":"Guangdong Provincial Laboratory of Chemistry and Fine Chemical Engineering Jieyang Center , ,","place":["Jieyang, China, 515200"]},{"name":"Guangdong University of Technology , , ,","place":["Guangzhou, China, 510006"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5437-6992","authenticated-orcid":true,"given":"Qiaozhi","family":"Ma","sequence":"additional","affiliation":[{"name":"South China Agricultural University , , ,","place":["Guangzhou, China, 510642"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8765-7061","authenticated-orcid":true,"given":"Xueqing","family":"Qiu","sequence":"additional","affiliation":[{"name":"Guangdong University of Technology , , ,","place":["Guangzhou, China, 510006"]},{"name":"Guangdong Provincial Laboratory of Chemistry and Fine Chemical Engineering Jieyang Center , ,","place":["Jieyang, China, 515200"]},{"name":"Guangdong University of Technology , , ,","place":["Guangzhou, China, 510006"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,7,27]]},"reference":[{"issue":"6185","key":"2026080510092657000_cit1","doi-asserted-by":"publisher","DOI":"10.1126\/science.1246843","article-title":"Lignin Valorization: Improving Lignin Processing in\nthe Biorefinery","volume":"344","author":"Ragauskas","year":"2014","journal-title":"Science"},{"issue":"14","key":"2026080510092657000_cit2","doi-asserted-by":"publisher","first-page":"6778","DOI":"10.1021\/acssuschemeng.5c14139","article-title":"Intermolecular\nForce Quantification for Deciphering Lignin Dissolution Behavior in\nSolvents","volume":"14","author":"Liu","year":"2026","journal-title":"ACS Sustainable Chem. 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