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We report a nickel\/photoredox-catalyzed coupling of 1,3-butadiene, aldehydes, and aryl bromides using Hantzsch ester as an organic reductant. The reaction proceeds under mild conditions with high regio- and stereoselectivity and broad functional-group tolerance. Control experiments and DFT calculations support a pathway involving nickel photoreduction, butadiene insertion, and carbonyl addition of a nucleophilic \u03c0-allylnickel intermediate.<\/jats:p>","DOI":"10.1021\/acs.joc.6c01104","type":"journal-article","created":{"date-parts":[[2026,8,4]],"date-time":"2026-08-04T13:12:15Z","timestamp":1785849135000},"page":"10774-10779","source":"Crossref","is-referenced-by-count":0,"title":["Nickel\/Photoredox\nThree-Component Coupling of 1,3-Butadiene,\nAldehydes, and Aryl Bromides to Homoallylic Alcohols"],"prefix":"10.1021","volume":"91","author":[{"given":"Shuto","family":"Odagaki","sequence":"first","affiliation":[{"name":"Kwansei Gakuin University , , , ,","place":["Sanda, Hyogo, Japan, 669-1337"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tomohiro","family":"Yoshida","sequence":"additional","affiliation":[{"name":"Kwansei Gakuin University , , , ,","place":["Sanda, Hyogo, Japan, 669-1337"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8417-7660","authenticated-orcid":true,"given":"Takuya","family":"Kurahashi","sequence":"additional","affiliation":[{"name":"Kwansei Gakuin University , , , ,","place":["Sanda, Hyogo, Japan, 669-1337"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,7,28]]},"reference":[{"key":"2026080708075860200_cit1","doi-asserted-by":"publisher","first-page":"1447","DOI":"10.1039\/D4RA06681B","article-title":"Multicomponent Reactions (MCRs) Yielding Medicinally\nRelevant Rings: A Recent Update and Chemical Space Analysis of the\nScaffolds","volume":"15","author":"Tandi","year":"2025","journal-title":"RSC Adv."},{"key":"2026080708075860200_cit2a","doi-asserted-by":"publisher","first-page":"436","DOI":"10.1021\/jacs.9b11178","article-title":"A Catalytic\nApproach for Enantioselective Synthesis of Homoallylic Alcohols Bearing\na Z-Alkenyl Chloride or Trifluoromethyl Group. 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