{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,8,7]],"date-time":"2026-08-07T17:13:46Z","timestamp":1786122826353,"version":"build-2736575974"},"reference-count":55,"publisher":"American Chemical Society (ACS)","issue":"31","license":[{"start":{"date-parts":[[2026,7,24]],"date-time":"2026-07-24T00:00:00Z","timestamp":1784851200000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-029"},{"start":{"date-parts":[[2026,7,24]],"date-time":"2026-07-24T00:00:00Z","timestamp":1784851200000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-037"},{"start":{"date-parts":[[2026,7,24]],"date-time":"2026-07-24T00:00:00Z","timestamp":1784851200000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-045"}],"funder":[{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["NSFC-22371228"],"award-info":[{"award-number":["NSFC-22371228"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,8,7]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>Carbonyl desaturation represents a fundamental chemical transformation widely practiced in organic synthesis. Transition metal-catalyzed direct \u03b1,\u03b2-desaturation of carbonyl compounds has been well developed. Herein, we disclose an efficient one-pot synthesis of flavones from phenolic ketones via double iodine-catalyzed \u03b1,\u03b2-dehydrogenation and an oxa-Michael addition. This protocol is a metal-free approach to carbonyl desaturation with nontoxic DMSO as both the solvent and oxidant, which is especially beneficial for the synthesis of pharmaceutical compounds. Mechanistic studies suggest that the transformation proceeds via a radical pathway.<\/jats:p>","DOI":"10.1021\/acs.joc.6c01237","type":"journal-article","created":{"date-parts":[[2026,7,27]],"date-time":"2026-07-27T04:59:59Z","timestamp":1785128399000},"page":"10702-10708","source":"Crossref","is-referenced-by-count":0,"title":["Iodine-Catalyzed Carbonyl\nDesaturation: A One-Pot\nSynthesis of Flavones"],"prefix":"10.1021","volume":"91","author":[{"given":"Heng-Xin","family":"Mao","sequence":"first","affiliation":[{"name":"Northwest University , , ,","place":["Xi\u2019an, China, 710069"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bao-Yin","family":"Zhao","sequence":"additional","affiliation":[{"name":"Northwest University , , ,","place":["Xi\u2019an, China, 710069"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Li-Gang","family":"Kou","sequence":"additional","affiliation":[{"name":"Northwest University , , ,","place":["Xi\u2019an, China, 710069"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bin-Xuan","family":"Zou","sequence":"additional","affiliation":[{"name":"Northwest University , , ,","place":["Xi\u2019an, China, 710069"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2774-3248","authenticated-orcid":true,"given":"Yong-Qiang","family":"Wang","sequence":"additional","affiliation":[{"name":"Northwest University , , ,","place":["Xi\u2019an, China, 710069"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,7,24]]},"reference":[{"key":"2026080708080907400_cit1","doi-asserted-by":"publisher","first-page":"8201","DOI":"10.1021\/acscatal.6b02406","article-title":"Palladium-catalyzed aerobic dehydrogenation of cyclic\nhydrocarbons for the synthesis of substituted aromatics and other\nunsaturated products","volume":"6","author":"Iosub","year":"2016","journal-title":"ACS Catal."},{"key":"2026080708080907400_cit2","doi-asserted-by":"publisher","first-page":"622","DOI":"10.1016\/j.bmc.2005.08.036","article-title":"Cytotoxic activity of (S)-goniothalamin and analogues\nagainst human cancer cells","volume":"14","author":"de Fa\u0301tima","year":"2006","journal-title":"Biorg. 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Chem."},{"key":"2026080708080907400_cit50","doi-asserted-by":"publisher","first-page":"258","DOI":"10.1021\/acs.orglett.3c03925","article-title":"Enantioselective \u03b1-amination of amides by one-pot organo-\/iodine sequential\ncatalysis","volume":"26","author":"Bai","year":"2024","journal-title":"Org. Lett."},{"key":"2026080708080907400_cit51","doi-asserted-by":"publisher","first-page":"7881","DOI":"10.1021\/acs.joc.1c00861","article-title":"Iodine-Catalyzed\nMethylthiolative Annulation of 2-Alkynyl\nBiaryls with DMSO: A Metal-Free Approach to 9-Sulfenylphenanthrenes","volume":"86","author":"Mukherjee","year":"2021","journal-title":"J. Org. 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