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This multicomponent reaction proceeded under mild conditions to afford a range of dithiophosphinates using elemental sulfur as the sulfur source. The present photochemical protocol offers a sustainable and practical strategy for dithiophosphinate synthesis without transition metals or complex operational procedures.<\/jats:p>","DOI":"10.1021\/acs.joc.6c01346","type":"journal-article","created":{"date-parts":[[2026,8,4]],"date-time":"2026-08-04T13:06:20Z","timestamp":1785848780000},"page":"10738-10746","source":"Crossref","is-referenced-by-count":2,"title":["Visible-Light-Initiated\nFour-Component Reaction of\n\u03b1-Diazoesters, Cyclic Ethers, Elemental Sulfur, and Secondary\nPhosphines"],"prefix":"10.1021","volume":"91","author":[{"ORCID":"https:\/\/orcid.org\/0009-0003-9634-304X","authenticated-orcid":true,"given":"Yufen","family":"Lv","sequence":"first","affiliation":[{"name":"Qinghai Normal University , , , ,","place":["Xining, Qinghai, China, 810008"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jian","family":"Huang","sequence":"additional","affiliation":[{"name":"Qinghai Normal University , , , ,","place":["Xining, Qinghai, China, 810008"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4457-3233","authenticated-orcid":true,"given":"Huilan","family":"Yue","sequence":"additional","affiliation":[{"name":"Northwest Institute of Plateau Biology , , , ,","place":["Xining, Qinghai, P. 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