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This strategy utilizes commercially available and industrially applicable Se powder as the building block for selenium-containing motifs, circumventing the need for selenyl precursors that are toxic, unstable, and difficult to store. A wide range of arylboronic acids, including sterically congested boronic acids, are smoothly accommodated with this method. The potential synthetic utility is highlighted by its operational simplicity, extensive substrate scope, good functional group compatibility, gram-scale synthesis, and transformations. Furthermore, preliminary mechanistic experiments revealed that a radical pathway is integrated in this transformation.<\/jats:p>","DOI":"10.1021\/acs.joc.6c01518","type":"journal-article","created":{"date-parts":[[2026,9,3]],"date-time":"2026-09-03T02:10:26Z","timestamp":1788401426000},"page":"12344-12353","source":"Crossref","is-referenced-by-count":2,"title":["Three-Component\nRadical C\u2013H Selenylation of\n                    <i>N<\/i>\n                    -Acyl\nAnilines under Metal-Free Conditions"],"prefix":"10.1021","volume":"91","author":[{"given":"Quanrui","family":"Yao","sequence":"first","affiliation":[{"name":"University of South China , , , ,","place":["Hengyang, Hunan, China, 421001"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zijing","family":"Xing","sequence":"additional","affiliation":[{"name":"University of South China , , , ,","place":["Hengyang, Hunan, China, 421001"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhouting","family":"Zeng","sequence":"additional","affiliation":[{"name":"University of South China , , , ,","place":["Hengyang, Hunan, China, 421001"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ziyou","family":"Tang","sequence":"additional","affiliation":[{"name":"University of South China , , , ,","place":["Hengyang, Hunan, China, 421001"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yaqian","family":"Li","sequence":"additional","affiliation":[{"name":"Changsha Medical University , , ,","place":["Changsha, China, 410219"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Honggui","family":"Huang","sequence":"additional","affiliation":[{"name":"Renmin Hospital of Wuhan University , , ,","place":["Wuhan, China, 430060"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7624-5499","authenticated-orcid":true,"given":"Jinhui","family":"Cai","sequence":"additional","affiliation":[{"name":"University of South China , , , ,","place":["Hengyang, Hunan, China, 421001"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,31]]},"reference":[{"key":"2026091109112293600_cit1a","doi-asserted-by":"publisher","first-page":"5386","DOI":"10.1002\/adsc.202101227","article-title":"Synthesis of Organoselenium\nCompounds with Elemental Selenium","volume":"363","author":"Ma","year":"2021","journal-title":"Adv. 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