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Herein, surface-treated indium phosphide (InP) QDs with tetrapod and tetrahedral morphologies were synthesized through a temperature-controlled hot-injection method followed by hydrofluoric acid post-treatment. Removal of the native surface oxide layer effectively suppresses charge-carrier trapping and prolongs carrier lifetimes, resulting in significantly enhanced photocatalytic CO2 reduction activity. More importantly, the product selectivity is governed by the exposed crystal facets: (110)-oriented tetrapod preferentially produces CO through a two-electron pathway, whereas (111)-oriented tetrahedron promotes further hydrogenation toward CH4. This work establishes a direct structure\u2013reactivity relationship between surface atomic arrangement and CO2 photoreduction selectivity, providing a design principle for environmentally benign QD photocatalysts for solar fuel production.<\/jats:p>","DOI":"10.1021\/acs.jpclett.6c02570","type":"journal-article","created":{"date-parts":[[2026,9,28]],"date-time":"2026-09-28T19:01:50Z","timestamp":1790622110000},"page":"11553-11561","source":"Crossref","is-referenced-by-count":0,"title":["Surface-Treated\nInP Quantum Dots for Selective CO2 Photoreduction"],"prefix":"10.1021","volume":"17","author":[{"given":"Le-Chun","family":"Li","sequence":"first","affiliation":[{"name":"National University of Tainan , , ,","place":["Tainan, Taiwan, 700301"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chia-Ying","family":"Wu","sequence":"additional","affiliation":[{"name":"Feng Chia University , , ,","place":["Taichung, Taiwan, 40724"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tsukasa","family":"Takanashi","sequence":"additional","affiliation":[{"name":"University of Toyama , , 3190 Gofuku , ,","place":["Toyama, Japan, 930-8555"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0001-6823-2612","authenticated-orcid":true,"given":"Shih-Wen","family":"Tseng","sequence":"additional","affiliation":[{"name":"Core Facility Center of National Cheng Kung University , ,","place":["Tainan, Taiwan, 70101"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7371-204X","authenticated-orcid":true,"given":"Tetsu","family":"Yonezawa","sequence":"additional","affiliation":[{"name":"Hokkaido University , , ,","place":["Hokkaido, Japan, 060-8628"]},{"name":"Chulalongkorn University , , ,","place":["Bangkok, Thailand, 10330"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3179-7588","authenticated-orcid":true,"given":"Akira","family":"Yamakata","sequence":"additional","affiliation":[{"name":"Okayama University , , ,","place":["Okayama, Japan, 700-8530"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5665-6496","authenticated-orcid":true,"given":"Chen-Hao","family":"Yeh","sequence":"additional","affiliation":[{"name":"Feng Chia University , , ,","place":["Taichung, Taiwan, 40724"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-0685-7200","authenticated-orcid":true,"given":"Ying-Chih","family":"Pu","sequence":"additional","affiliation":[{"name":"National University of Tainan , , ,","place":["Tainan, Taiwan, 700301"]},{"name":"National Sun Yat-sen University , , ,","place":["Kaohsiung, Taiwan, 80424"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,28]]},"reference":[{"issue":"6","key":"2026100811155809800_cit1","doi-asserted-by":"publisher","first-page":"75","DOI":"10.1007\/s11783-024-1835-0","article-title":"Recent Advances, Challenges, and Perspectives on Carbon Capture","volume":"18","author":"Zhang","year":"2024","journal-title":"Front. 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