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Existing colloidal syntheses of CsPbI3 predominantly produce nanocubes or other hexahedral shapes because of the stability of the nanocube facets in the perovskite structure. In this work, we utilize a bidentate ammonium ligand with a tunable linker between the two head groups in order to preferentially nucleate and stabilize rhombic dodecahedral nanocrystals. These particles show enhanced environmental stability compared to CsPbI3 nanocrystals capped with monodentate ammonium ligands and self-assemble into ordered, hexagonally packed monolayers. This work represents a new entry into the limited shape catalog of CsPbI3 and expands the design principles for facet-selective ligands in lead-halide perovskite nanocrystals.<\/jats:p>","DOI":"10.1021\/acs.nanolett.6c03385","type":"journal-article","created":{"date-parts":[[2026,9,23]],"date-time":"2026-09-23T14:01:57Z","timestamp":1790172117000},"page":"13442-13449","source":"Crossref","is-referenced-by-count":0,"title":["Synthesis of\nCsPbI3 Rhombic Dodecahedra\nUsing Facet-Selective Bidentate Ammonium Ligands"],"prefix":"10.1021","volume":"26","author":[{"given":"Nicholas","family":"Favate","sequence":"first","affiliation":[{"name":"Purdue University , , , ,","place":["West Lafayette, Indiana, United States, 47907"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Emma","family":"Daggett","sequence":"additional","affiliation":[{"name":"Purdue University , , , ,","place":["West Lafayette, Indiana, United States, 47907"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zihang","family":"Liu","sequence":"additional","affiliation":[{"name":"Beijing Normal University , , ,","place":["Beijing, People\u2019s Republic of China, 100875"]},{"name":"Anhui University , , ,","place":["Hefei, People\u2019s Republic of China, 230601"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Sarah M.","family":"Kolp","sequence":"additional","affiliation":[{"name":"Purdue University , , , ,","place":["West Lafayette, Indiana, United States, 47907"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3912-8899","authenticated-orcid":true,"given":"Run","family":"Long","sequence":"additional","affiliation":[{"name":"Beijing Normal University , , ,","place":["Beijing, People\u2019s Republic of China, 100875"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5140-7500","authenticated-orcid":true,"given":"Oleg V.","family":"Prezhdo","sequence":"additional","affiliation":[{"name":"University of New Mexico , , , ,","place":["Albuquerque, New Mexico, United States, 87106"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7566-4475","authenticated-orcid":true,"given":"Jonathan D.","family":"Hood","sequence":"additional","affiliation":[{"name":"Purdue University , , , ,","place":["West Lafayette, Indiana, United States, 47907"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3538-9955","authenticated-orcid":true,"given":"Christina W.","family":"Li","sequence":"additional","affiliation":[{"name":"Purdue University , , , ,","place":["West Lafayette, Indiana, United States, 47907"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,23]]},"reference":[{"key":"2026100710102807600_cit1","doi-asserted-by":"publisher","first-page":"3692","DOI":"10.1021\/nl5048779","article-title":"Nanocrystals\nof Cesium Lead Halide Perovskites (CsPbX3, X = Cl, Br,\nand I): Novel Optoelectronic Materials Showing Bright Emission with\nWide Color Gamut","volume":"15","author":"Protesescu","year":"2015","journal-title":"Nano Lett."},{"key":"2026100710102807600_cit2","doi-asserted-by":"publisher","first-page":"7382","DOI":"10.1021\/acs.nanolett.0c02784","article-title":"Thermal\nDecoherence of Superradiance in Lead Halide Perovskite Nanocrystal\nSuperlattices","volume":"20","author":"Mattiotti","year":"2020","journal-title":"Nano Lett."},{"key":"2026100710102807600_cit3","doi-asserted-by":"publisher","first-page":"7811","DOI":"10.1021\/acs.nanolett.2c02427","article-title":"Superradiance\nand Exciton Delocalization in Perovskite Quantum Dot Superlattices","volume":"22","author":"Blach","year":"2022","journal-title":"Nano Lett."},{"key":"2026100710102807600_cit4","doi-asserted-by":"publisher","first-page":"671","DOI":"10.1038\/s41586-018-0683-0","article-title":"Superfluorescence from\nlead halide perovskite quantum\ndot superlattices","volume":"563","author":"Raino","year":"2018","journal-title":"Nature"},{"key":"2026100710102807600_cit5","doi-asserted-by":"publisher","first-page":"489","DOI":"10.1021\/acs.jpclett.6b02800","article-title":"High Defect Tolerance\nin Lead Halide Perovskite CsPbBr3","volume":"8","author":"Kang","year":"2017","journal-title":"J. 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