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Introducing oxophilic species into Pt catalysts can mitigate this poisoning by promoting the oxidation of adsorbed CO via OH* generated on such species. However, rational construction of Pt\u2013oxophilic heterojunctions is often hindered by their significant lattice mismatch. Here, amorphous BiSx-decorated porous Pt nanorods (a-BiSx\/Pt NRs) are prepared through acid etching of Pt2Bi2\/Pt NRs, which are templated by Bi2S3 nanorods. The resulting a-BiSx\/Pt NRs exhibit a mass activity of 2.05 A mgPt\u20131 for acidic MOR, which is 12.8 times higher than that of commercial Pt\/C (0.16 A mgPt\u20131). In situ infrared spectroscopy and density functional theory calculations reveal that the a-BiSx\u2013Pt heterointerface synergistically weakens CO adsorption on Pt via electronic modification and promotes OH* generation through the bifunctional mechanism of oxophilic Bi sites, thereby facilitating the oxidative removal of CO intermediates and enhancing MOR performance.<\/jats:p>","DOI":"10.1021\/acs.nanolett.6c03420","type":"journal-article","created":{"date-parts":[[2026,9,10]],"date-time":"2026-09-10T08:01:13Z","timestamp":1789027273000},"page":"12519-12526","source":"Crossref","is-referenced-by-count":0,"title":["Synergistic\nElectronic and Bifunctional Effects in\nAmorphous BiS\n                    <i>x<\/i>\n                    -Decorated Porous\nPt Nanorods for CO-Tolerant Methanol Oxidation"],"prefix":"10.1021","volume":"26","author":[{"given":"Lijun","family":"Hu","sequence":"first","affiliation":[{"name":"Nanjing University , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Heyu","family":"Sui","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yan","family":"Wang","sequence":"additional","affiliation":[{"name":"Nanjing University , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Li","family":"Zhai","sequence":"additional","affiliation":[{"name":"City University of Hong Kong , , ,","place":["Hong Kong, China, 999077"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yue","family":"Chen","sequence":"additional","affiliation":[{"name":"Nanjing University , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Haixia","family":"Liu","sequence":"additional","affiliation":[{"name":"Nanjing University , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jiuyi","family":"Hu","sequence":"additional","affiliation":[{"name":"Nanjing University , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4650-5226","authenticated-orcid":true,"given":"Yuanmiao","family":"Sun","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0470-8415","authenticated-orcid":true,"given":"Xue-Jun","family":"Wu","sequence":"additional","affiliation":[{"name":"Nanjing University , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,10]]},"reference":[{"key":"2026092309474570700_cit1","doi-asserted-by":"publisher","first-page":"2103505","DOI":"10.1002\/aenm.202103505","article-title":"Multiple Twin Boundary-Regulated Metastable Pd for Ethanol Oxidation\nReaction","volume":"12","author":"Liu","year":"2022","journal-title":"Adv. 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Funct. Mater."},{"key":"2026092309474570700_cit28","doi-asserted-by":"publisher","first-page":"2418890","DOI":"10.1002\/adma.202418890","article-title":"High-Entropy Metal Sulfide Nanocrystal Libraries for Highly Reversible\nSodium Storage","volume":"37","author":"Zhang","year":"2025","journal-title":"Adv. Mater."},{"key":"2026092309474570700_cit29","doi-asserted-by":"publisher","first-page":"386","DOI":"10.1039\/C4NR05778C","article-title":"Correlation of the\nStructure and Applications of Dealloyed Nanoporous Metals in Catalysis\nand Energy Conversion\/Storage","volume":"7","author":"Qiu","year":"2015","journal-title":"Nanoscale"},{"key":"2026092309474570700_cit30","doi-asserted-by":"publisher","first-page":"162","DOI":"10.1002\/cmtd.202000069","article-title":"In Situ X-ray Absorption\nSpectroscopy of Platinum Electrocatalysts","volume":"1","author":"Morris","year":"2021","journal-title":"Chem.\nMethods"},{"key":"2026092309474570700_cit31","doi-asserted-by":"publisher","first-page":"80","DOI":"10.1007\/s40820-023-01282-4","article-title":"Interfacial Electronic Modulation of Dual-Monodispersed\nPt\u2013Ni3S2 as Efficacious Bi-Functional\nElectrocatalysts for Concurrent H2 Evolution and Methanol\nSelective Oxidation","volume":"16","author":"Zhao","year":"2024","journal-title":"Nano-Micro Lett."},{"key":"2026092309474570700_cit32","doi-asserted-by":"publisher","DOI":"10.1002\/advs.202510123","article-title":"Femtosecond-Laser Synthesized\nPtBi Nanoalloys for Efficient Methanol Oxidation in Hybrid Electrolysis","volume":"12","author":"Zhang","year":"2025","journal-title":"Adv. Sci."},{"key":"2026092309474570700_cit33","doi-asserted-by":"publisher","DOI":"10.1016\/j.apsusc.2023.157782","article-title":"Low-Coordinated Platinum\nMaterial for Hydrogenation of m-Dinitrobenzene to m-Phenylenediamine","volume":"636","author":"Ji","year":"2023","journal-title":"Appl. Surf. Sci."},{"key":"2026092309474570700_cit34","doi-asserted-by":"publisher","first-page":"7588","DOI":"10.1021\/acsaem.0c01028","article-title":"Aqueous\nSynthesis of Highly Dispersed Pt2Bi Alloy Nanoplatelets\nfor Dimethyl Ether Electro-Oxidation","volume":"3","author":"Tonnis","year":"2020","journal-title":"ACS Appl.\nEnergy Mater."},{"key":"2026092309474570700_cit35","doi-asserted-by":"publisher","first-page":"23046","DOI":"10.1021\/acsami.0c06460","article-title":"Tunable Hollow\nPt@Ru Dodecahedra via Galvanic Replacement for Efficient Methanol\nOxidation","volume":"12","author":"Bai","year":"2020","journal-title":"ACS Appl. Mater. Interfaces"},{"key":"2026092309474570700_cit36","doi-asserted-by":"publisher","first-page":"7675","DOI":"10.1002\/anie.202014144","article-title":"Synthesis\nof Core@Shell Cu-Ni@Pt-Cu Nano-Octahedra and Their Improved MOR Activity","volume":"60","author":"Li","year":"2021","journal-title":"Angew. Chem. Int. Ed."},{"key":"2026092309474570700_cit37","doi-asserted-by":"publisher","first-page":"5890","DOI":"10.1021\/jacs.7b01482","article-title":"Synthesis of Low Pt-Based Quaternary PtPdRuTe Nanotubes with Optimized\nIncorporation of Pd for Enhanced Electrocatalytic Activity","volume":"139","author":"Ma","year":"2017","journal-title":"J. Am. Chem. Soc."},{"key":"2026092309474570700_cit38","doi-asserted-by":"publisher","DOI":"10.1002\/admt.202501383","article-title":"Thermally\nTreated MoO3 Supports for Pt\/C Catalysts: Enhancing the\nMethanol Electro-Oxidation Efficiency","volume":"11","author":"Sekhar","year":"2026","journal-title":"Adv.\nMater. 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Sci."},{"key":"2026092309474570700_cit45","doi-asserted-by":"publisher","first-page":"2500402","DOI":"10.1002\/smll.202500402","article-title":"Stereo Assembly\nof Bimetallic PtPd on Ti3C2Tx\/PProDOT\nfor Efficient Methanol Oxidation Reaction in Both Acidic and Alkaline\nMedia","volume":"21","author":"Xie","year":"2025","journal-title":"Small"},{"key":"2026092309474570700_cit46","doi-asserted-by":"publisher","first-page":"2307283","DOI":"10.1002\/smll.202307283","article-title":"A Universal Approach\nfor Controllable Synthesis of Homogeneously Alloyed PtM Nanoflowers\ntoward Enhanced Methanol Oxidation","volume":"20","author":"Qiao","year":"2024","journal-title":"Small"},{"key":"2026092309474570700_cit47","doi-asserted-by":"publisher","first-page":"13756","DOI":"10.1021\/acs.nanolett.5c02842","article-title":"Unraveling the Origin of Nb-Doped\nPt Nanoparticle Electrocatalysts for the Methanol Oxidation Reaction","volume":"25","author":"Zhang","year":"2025","journal-title":"Nano Lett."},{"key":"2026092309474570700_cit48","doi-asserted-by":"publisher","first-page":"5513","DOI":"10.1021\/acssuschemeng.5c11985","article-title":"Highly Efficient Anti-CO Poisoning Catalyst by Coupling\nMo 4d\u2013Ce\n4f Electronic States to Regulate the Electronic Structure of Pt","volume":"14","author":"Cheng","year":"2026","journal-title":"ACS Sustainable Chem. Eng."},{"key":"2026092309474570700_cit49","doi-asserted-by":"publisher","first-page":"1635","DOI":"10.1038\/s41467-026-68352-0","article-title":"Interphase Electron\nRedistribution Induced by Confined Transformation\nin PtPdBiSn Nanoplates for Efficient Ethanol Oxidation Electrocatalysis","volume":"17","author":"Shao","year":"2026","journal-title":"Nat. Commun."},{"key":"2026092309474570700_cit50","doi-asserted-by":"publisher","first-page":"15034","DOI":"10.3390\/ijms232315034","article-title":"Pt-Based Nanostructures\nfor Electrochemical\nOxidation of CO: Unveiling the Effect of Shapes and Electrolytes","volume":"23","author":"Abdelgawad","year":"2022","journal-title":"Int. J. Mol. Sci."},{"key":"2026092309474570700_cit51","doi-asserted-by":"publisher","first-page":"12145","DOI":"10.1021\/jacs.1c04315","article-title":"Triggering Water and\nMethanol Activation for Solar-Driven H2 Production: Interplay\nof Dual Active Sites over Plasmonic ZnCu Alloy","volume":"143","author":"Luo","year":"2021","journal-title":"J. Am. Chem. Soc."},{"key":"2026092309474570700_cit52","doi-asserted-by":"publisher","first-page":"3324","DOI":"10.1038\/s41467-021-23696-7","article-title":"Unique Structure of Active Platinum-Bismuth Site for\nOxidation of Carbon Monoxide","volume":"12","author":"Nan","year":"2021","journal-title":"Nat. Commun."},{"key":"2026092309474570700_cit53","doi-asserted-by":"publisher","first-page":"13783","DOI":"10.1021\/acssuschemeng.5c03711","article-title":"Materializing\nEfficient Collaborative Multifunctional Electrocatalysis via the Electron\nDelocalization Effect between Pt and Substrate","volume":"13","author":"Xiong","year":"2025","journal-title":"ACS Sustainable Chem. 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