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In this study, the core skeleton is synthesized via an electrochemical method utilizing commercially available acids and easily accessible hydrazones through an iodination-triggered reaction. This approach broadens the substrate scope under mild reaction conditions. Mechanistic studies indicate that the reaction proceeds via an iodination-triggered reaction between hydrazones and acids to generate an intermediate, which subsequently undergoes Mumm rearrangement to afford the desired products.<\/jats:p>","DOI":"10.1021\/acs.orglett.6c02737","type":"journal-article","created":{"date-parts":[[2026,7,17]],"date-time":"2026-07-17T19:04:33Z","timestamp":1784315073000},"page":"9805-9810","source":"Crossref","is-referenced-by-count":0,"title":["Electrochemical\nIodination-Triggered Mumm Rearrangement\nof Hydrazones with Acids: Access to\n                    <i>N,N<\/i>\n                    \u2032-Diacylhydrazines"],"prefix":"10.1021","volume":"28","author":[{"given":"Yongzheng","family":"Yin","sequence":"first","affiliation":[{"name":"East China University of Science and Technology , , ,","place":["Shanghai, P. R. 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