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Merging 1,2-carbonyl migration and radical-polar crossover, this protocol delivers a variety of valuable fluorine-containing acetamides and features broad substrate compatibility, including natural product and pharmaceutical skeletons. Gram-scale synthesis, product derivatization and AIE properties are demonstrated. Mechanistic control experiments including radical trapping, deuterium labeling, and luminescence quenching studies collectively support a catalytic cycle involving photoinduced single-electron transfer, intramolecular 1,2-carbonyl migration, and subsequent ionic nucleophilic capture through radical-polar crossover.<\/jats:p>","DOI":"10.1021\/acs.orglett.6c03083","type":"journal-article","created":{"date-parts":[[2026,9,3]],"date-time":"2026-09-03T18:51:09Z","timestamp":1788461469000},"page":"11500-11505","source":"Crossref","is-referenced-by-count":1,"title":["Photoredox-Catalyzed\nTrifunctionalization of\n                    <i>\u03b2,\u03b3<\/i>\n                    -Unsaturated\nKetones Enabled by Four-Component\n1,2-Carbonyl Migration\/Radical-Polar Crossover Cascade"],"prefix":"10.1021","volume":"28","author":[{"given":"Jia-Wen","family":"Liu","sequence":"first","affiliation":[{"name":"Changzhou University , , , ,","place":["Changzhou, Jiangsu, P. R. 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