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A series of substituted (1,2b)-syn-2-hydroxy-1-aryl-2-tetrahydroisoquinolin propan-1-ones were obtained with moderate to excellent yields and excellent selectivities (syn:anti &amp;gt;19:1). In addition, density functional theory (DFT) calculations were performed to explain the stereochemistry outcome for this novel transformation.<\/jats:p>","DOI":"10.1021\/acs.orglett.6c03259","type":"journal-article","created":{"date-parts":[[2026,9,4]],"date-time":"2026-09-04T16:01:58Z","timestamp":1788537718000},"page":"11620-11625","source":"Crossref","is-referenced-by-count":0,"title":["Micro Water-Initiated\nand Cu(OTf)2-Catalyzed\nOxygen Transfer-Insertion-Mannich-Type Reaction of\n                    <i>\u03b1<\/i>\n                    -Carbonyl Diazos with Benzo-\n                    <i>N<\/i>\n                    ,\n                    <i>O<\/i>\n                    -acetals"],"prefix":"10.1021","volume":"28","author":[{"given":"Xin","family":"Li","sequence":"first","affiliation":[{"name":"Fudan University , , ,","place":["Shanghai, China, 201203"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jian-Ting","family":"Sun","sequence":"additional","affiliation":[{"name":"Fudan University , , ,","place":["Shanghai, China, 201203"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yu","family":"Zhang","sequence":"additional","affiliation":[{"name":"Fudan University , , ,","place":["Shanghai, China, 201203"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yu-Ying","family":"Zhang","sequence":"additional","affiliation":[{"name":"Fudan University , , ,","place":["Shanghai, China, 201203"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1488-7311","authenticated-orcid":true,"given":"Jian-Liang","family":"Ye","sequence":"additional","affiliation":[{"name":"Xiamen University , , , ,","place":["Xiamen, Fujian, China, 361005"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3470-6741","authenticated-orcid":true,"given":"Bang-Guo","family":"Wei","sequence":"additional","affiliation":[{"name":"Fudan University , , ,","place":["Shanghai, China, 201203"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,4]]},"reference":[{"key":"2026091809425682000_cit1a","doi-asserted-by":"publisher","first-page":"7453","DOI":"10.1038\/s41467-025-62706-w","article-title":"Catalyst-free\nUllmann coupling in aqueous microdroplets","volume":"16","author":"Jia","year":"2025","journal-title":"Nat.\nCommun."},{"key":"2026091809425682000_cit1b","doi-asserted-by":"publisher","DOI":"10.1016\/j.chempr.2025.102552","article-title":"Syngas chemistry:\nRational design of tandem reaction pathway for directional hydrocarbon\nsynthesis","volume":"11","author":"Su","year":"2025","journal-title":"Chem."},{"key":"2026091809425682000_cit1c","doi-asserted-by":"publisher","first-page":"112","DOI":"10.1038\/s41586-025-08887-2","article-title":"Generalizing arene C-H alkylations\nby radical-radical cross-coupling","volume":"641","author":"Gro\u00dfkopf","year":"2025","journal-title":"Nature"},{"key":"2026091809425682000_cit2a","doi-asserted-by":"publisher","DOI":"10.1002\/anie.202518689","article-title":"Ph2SCCO:\nA new versatile\nCCO-fragment transfer reagent","volume":"64","author":"Sun","year":"2025","journal-title":"Angew. 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