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Herein, a symmetrical BODIPY bis(oxime ester) derivative (BD-diOE) was developed for visible-light-triggered release of valproic acid (VPA). The study confirmed a sequential photo-uncaging process resulting in the release of two equivalents of VPA. To improve aqueous performance, BD-diOE was encapsulated into Pluronic F127 micelles (BD-diOE@F127). Quantitative analysis revealed that BD-diOE@F127 in water releases approximately 30% more VPA than BD-diOE in a methanol\u2013mixed water solvent under identical irradiation conditions. Moreover, BD-diOE@F127 exhibited pronounced light-dependent in vitro cytotoxicity. These results demonstrate that the combination of symmetric molecular design and micelle formulation provides a promising platform for photo-responsive biomaterials and controlled drug delivery applications.<\/jats:p>","DOI":"10.1021\/acsabm.6c01438","type":"journal-article","created":{"date-parts":[[2026,10,1]],"date-time":"2026-10-01T08:01:37Z","timestamp":1790841697000},"page":"9822-9830","source":"Crossref","is-referenced-by-count":0,"title":["Light-Induced Double Drug Release with Improved Efficiency in Micelles"],"prefix":"10.1021","volume":"9","author":[{"ORCID":"https:\/\/orcid.org\/0009-0000-2015-6246","authenticated-orcid":true,"given":"Xuemei","family":"Chen","sequence":"first","affiliation":[{"name":"New Jersey Institute of Technology , , 323 Martin Luther King Jr. Blvd , , ,","place":["Newark, New Jersey, United States, 07102"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bryan","family":"Liu","sequence":"additional","affiliation":[{"name":"New Jersey Institute of Technology , , 323 Martin Luther King Jr. Blvd , , ,","place":["Newark, New Jersey, United States, 07102"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yongqing","family":"Yang","sequence":"additional","affiliation":[{"name":"New Jersey Institute of Technology , , 323 Martin Luther King Jr. Blvd , , ,","place":["Newark, New Jersey, United States, 07102"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yanmei","family":"Li","sequence":"additional","affiliation":[{"name":"New Jersey Institute of Technology , , 323 Martin Luther King Jr. Blvd , , ,","place":["Newark, New Jersey, United States, 07102"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8090-8593","authenticated-orcid":true,"given":"Hao","family":"Chen","sequence":"additional","affiliation":[{"name":"New Jersey Institute of Technology , , 323 Martin Luther King Jr. Blvd , , ,","place":["Newark, New Jersey, United States, 07102"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhaohui","family":"Feng","sequence":"additional","affiliation":[{"name":"Rutgers Cancer Institute, Rutgers-State University of New Jersey , , , ,","place":["New Brunswick, New Jersey, United States, 08903"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2111-0981","authenticated-orcid":true,"given":"Yuanwei","family":"Zhang","sequence":"additional","affiliation":[{"name":"New Jersey Institute of Technology , , 323 Martin Luther King Jr. Blvd , , ,","place":["Newark, New Jersey, United States, 07102"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,10,1]]},"reference":[{"issue":"16","key":"2026101904071170100_cit1","doi-asserted-by":"publisher","first-page":"14878","DOI":"10.1039\/d5ra09767c","article-title":"Smart microdevices for biomedical drug delivery: endogenous stimuli as the key to safer therapeutics","volume":"16","author":"Datta","year":"2026","journal-title":"RSC Adv."},{"issue":"1","key":"2026101904071170100_cit2","doi-asserted-by":"publisher","first-page":"119","DOI":"10.1021\/cr300177k","article-title":"Photoremovable protecting groups in chemistry and biology: reaction mechanisms and efficacy","volume":"113","author":"Kl\u00e1n","year":"2013","journal-title":"Chem. 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