{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,8,17]],"date-time":"2026-08-17T12:25:46Z","timestamp":1786969546429,"version":"build-2736575974"},"reference-count":56,"publisher":"American Chemical Society (ACS)","issue":"30","license":[{"start":{"date-parts":[[2026,7,27]],"date-time":"2026-07-27T00:00:00Z","timestamp":1785110400000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100020950","name":"National Science and Technology Council","doi-asserted-by":"publisher","award":["114-2811-E-008-007"],"award-info":[{"award-number":["114-2811-E-008-007"]}],"id":[{"id":"10.13039\/501100020950","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100020950","name":"National Science and Technology Council","doi-asserted-by":"publisher","award":["NSTC 113-2221-E-008-011-MY3"],"award-info":[{"award-number":["NSTC 113-2221-E-008-011-MY3"]}],"id":[{"id":"10.13039\/501100020950","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100020950","name":"National Science and Technology Council","doi-asserted-by":"publisher","award":["NSTC 114-2221-E-008-021"],"award-info":[{"award-number":["NSTC 114-2221-E-008-021"]}],"id":[{"id":"10.13039\/501100020950","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,8,5]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>Maintaining ultralow metal-ion purity in process chemicals is crucial in semiconductor fabrication, where trace Fe3+ contamination can lead to dielectric breakdown, yield loss, and unintended doping. Inductively coupled plasma mass spectrometry (ICP-MS) provides excellent qualitative and quantitative sensitivity; however, it requires specialized infrastructure, is time-consuming and costly, and is not well suited for rapid on-site screening. Herein, we present a deferoxamine-B (DFO-B)-functionalized silicon nanowire field-effect transistor (SiNW-FET) engineered for the ultrasensitive, label-free detection of Fe3+ in semiconductor-grade chemicals. Mixed PEG self-assembled monolayers were modified with DFO-B via aldehyde\u2013amine coupling to form a stable, high-affinity chelation interface. In aqueous Fe3+ standards, the DFO-B-functionalized SiNW-FET exhibited a linear response from 10\u201315 to 10\u201311 M, with a practical LOD of 10\u201315 M and an above-Nernst sensitivity of \u201324 mV dec\u20131. In chemically complex matrices, the practical analytical boundary shifted upward, with reliable Fe3+ responses observed at approximately 10\u201312 M in a 23-element mixed-ion matrix and \u223c10\u201313 M in a highly diluted IPA-derived multi-element matrix. Mechanistic analysis rationalizes the above-Nernst response using an equivalent-circuit framework involving chelation-associated chemical capacitance, coordination-induced interfacial polarization, and protonation-state effects. The sensor showed preferential Fe3+ response under tested interferent conditions and remained operational in mixed-ion and highly diluted IPA-containing matrices, while also revealing matrix-dependent shifts in analytical performance. This work introduces a rapid on-site Fe3+ screening approach based on a portable and potentially in situ-compatible SiNW-FET platform that can complement ICP-MS for contamination assessment, while establishing a modular sensing interface that can be extended to other transition metals through ligand substitution. With integration into microfluidic sample handling and CMOS-compatible readout, this technology offers a portable, point-of-use Fe3+ screening through a discrete incubation\u2013rinse\u2013electrical readout workflow.<\/jats:p>","DOI":"10.1021\/acsami.6c05478","type":"journal-article","created":{"date-parts":[[2026,7,27]],"date-time":"2026-07-27T08:06:11Z","timestamp":1785139571000},"page":"41903-41916","source":"Crossref","is-referenced-by-count":0,"title":["Deferoxamine-B\u2013Functionalized Silicon Nanowire Field-Effect Transistor Interfaces for Ultralow-Concentration Fe3+ Detection in Semiconductor Process Chemicals"],"prefix":"10.1021","volume":"18","author":[{"given":"Bharath Kumar","family":"Yadlapalli","sequence":"first","affiliation":[{"name":"National Central University , , ,","place":["Zhongli, Taiwan, 32001"]},{"name":"National Central University , , ,","place":["Zhongli, Taiwan, 32001"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tzu-Chen","family":"Huang","sequence":"additional","affiliation":[{"name":"National Central University , , ,","place":["Zhongli, Taiwan, 32001"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1895-5385","authenticated-orcid":true,"given":"Yu-Hsiang","family":"Lee","sequence":"additional","affiliation":[{"name":"National Central University , , ,","place":["Zhongli, Taiwan, 32001"]},{"name":"National Central University , , ,","place":["Zhongli, Taiwan, 32001"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yu-Che","family":"Cheng","sequence":"additional","affiliation":[{"name":"National Central University , , ,","place":["Zhongli, Taiwan, 32001"]},{"name":"Cathay General Hospital , , ,","place":["Taipei, Taiwan, 10630"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9930-7605","authenticated-orcid":true,"given":"Wen-Yih","family":"Chen","sequence":"additional","affiliation":[{"name":"National Central University , , ,","place":["Zhongli, Taiwan, 32001"]},{"name":"Cathay General Hospital , , ,","place":["Taipei, Taiwan, 10630"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,7,27]]},"reference":[{"key":"2026081707101539900_cit1","doi-asserted-by":"publisher","first-page":"6834","DOI":"10.1039\/C9AN01437C","article-title":"Addressing the practicalities of anodic stripping voltammetry for heavy metal detection: a tutorial review","volume":"144","author":"Borrill","year":"2019","journal-title":"Analyst"},{"key":"2026081707101539900_cit2","doi-asserted-by":"publisher","first-page":"1","DOI":"10.3109\/10408449509089885","article-title":"Minamata Disease: Methylmercury Poisoning in Japan Caused by Environmental Pollution","volume":"25","author":"Harada","year":"1995","journal-title":"Crit. 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