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Here, we revisit this \u201climitation\u201d as an opportunity to explore whether ion beams can purposefully induce redox transformations that reveal chemical and structural information inaccessible by conventional means. Using a suite of mixed metal oxides (Ce\u2013Mo, Ni\/Co\u2013Mo, and Ce\u2013Ti), we demonstrate that ion beam exposure can drive controlled reduction processes that sensitively report on intrinsic redox stability and metal\u2013oxygen bonding and provide an alternative route by which to assess relative chemical and electronic changes, to otherwise costly and time-consuming synchrotron studies.<\/jats:p>","DOI":"10.1021\/acsami.6c07564","type":"journal-article","created":{"date-parts":[[2026,8,16]],"date-time":"2026-08-16T15:01:39Z","timestamp":1786892499000},"page":"45710-45719","source":"Crossref","is-referenced-by-count":0,"title":["X-ray and Ion-Beam Reduction Kinetics of Mixed Metal Oxides as an Informative Tool"],"prefix":"10.1021","volume":"18","author":[{"given":"Fatima","family":"Sajid","sequence":"first","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"University College London , , Gower Street , ,","place":["London, UK, WC1H 0AJ"]},{"name":"Quaid-i-Azam University (QAU) , , ,","place":["Islamabad, Pakistan, 45320"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Charalampos","family":"Drivas","sequence":"additional","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"Translational Research Hub, Cardiff University , , ,","place":["Cardiff, UK, CF24 4HQ"]},{"name":"UK Catalysis Hub, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Emila","family":"Duka","sequence":"additional","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"University College London , , Gower Street , ,","place":["London, UK, WC1H 0AJ"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hanna","family":"Bras-Genfoud","sequence":"additional","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"University College London , , Gower Street , ,","place":["London, UK, WC1H 0AJ"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Arthur","family":"Graf","sequence":"additional","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"Translational Research Hub, Cardiff University , , ,","place":["Cardiff, UK, CF24 4HQ"]},{"name":"VerSoX, Diamond Light Source , Harwell Science and Innovation Campus , ,","place":["Didcot, UK, OX11 0DE"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Merlin","family":"Liedtke","sequence":"additional","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"University College London , , Gower Street , ,","place":["London, UK, WC1H 0AJ"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6571-5731","authenticated-orcid":true,"given":"David J.","family":"Morgan","sequence":"additional","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"Translational Research Hub, Cardiff University , , ,","place":["Cardiff, UK, CF24 4HQ"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4522-2486","authenticated-orcid":true,"given":"Robert","family":"Palgrave","sequence":"additional","affiliation":[{"name":"HarwellXPS, Research Complex at Harwell, Rutherford Appleton Labs , Harwell Campus , ,","place":["Didcot, UK, OX11 0FA"]},{"name":"University College London , , Gower Street , ,","place":["London, UK, WC1H 0AJ"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3651-7314","authenticated-orcid":true,"given":"Christopher M. 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