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However, precise control over composition redistribution and phase evolution remains challenging for high-entropy alloy nanoparticles (HEA NPs) synthesized under ultrafast nonequilibrium conditions. Herein, we propose a controllable electrical explosion of wire (EEW) strategy to regulate the dynamic phase transformation of AlFeCoNiCu HEA NPs. During EEW, energy deposition regulates the phase-transition sequence, vapor\/plasma-phase mixing, and rapid nonequilibrium condensation of metal wires, enabling sufficient atomic\/ionic diffusion and redistribution to form HEA nanocrystals with tunable crystal-phase constitution. The optimized FCC\/BCC phase constitution promotes multicomponent solid-solution formation and reduces local compositional heterogeneity, while rapid EEW-induced nonequilibrium condensation freezes lattice distortion, phase interfaces, and defects. As a result, the optimized HEA NPs exhibit excellent electromagnetic wave absorption (EWA), with a minimum reflection loss of \u201355.71 dB and an effective absorption bandwidth of 7.30 GHz. They also show enhanced corrosion resistance, with a corrosion potential of \u20130.026 V. This work demonstrates that EEW offers a scalable nonequilibrium phase-engineering route for constructing high-performance HEA nanocrystals with integrated EWA and corrosion-resistant functions.<\/jats:p>","DOI":"10.1021\/acsami.6c08448","type":"journal-article","created":{"date-parts":[[2026,9,3]],"date-time":"2026-09-03T10:18:42Z","timestamp":1788430722000},"page":"49624-49639","source":"Crossref","is-referenced-by-count":0,"title":["Synergistic Dynamic Phase Transformation during Wire Electro-explosion Enables High-Entropy Alloys Nanoparticles with Efficient Electromagnetic Absorption"],"prefix":"10.1021","volume":"18","author":[{"given":"Liwen","family":"Liang","sequence":"first","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6438-7345","authenticated-orcid":true,"given":"Jian","family":"Wu","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin","family":"Li","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Huantong","family":"Shi","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xingwen","family":"Li","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Aici","family":"Qiu","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bosen","family":"Lei","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7835-1666","authenticated-orcid":true,"given":"Bin","family":"Wang","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chuncai","family":"Kong","sequence":"additional","affiliation":[{"name":"Xi\u2019an Jiaotong University , , ,","place":["Xi\u2019an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,1]]},"reference":[{"key":"2026091615070560800_cit1","doi-asserted-by":"publisher","DOI":"10.1002\/adma.202510009","article-title":"A Perspective on High-Entropy Oxides as Potential Electromagnetic Wave Absorbers","volume":"37","author":"Gao","year":"2025","journal-title":"Adv. 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