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In this work, we designed and fabricated a series of nitrogen-doped carbon-supported copper-cobalt nanoparticles (CuxCo-NC). A distinctive volcano-type dependence of catalytic activity on the Cu\/Co molar ratio was revealed, and a remarkable DMC space-time yield (STY) of 5.35 g g\u20131 cat\u00b7h\u20131 was delivered by the optimal composition (Cu\/Co = 3). There was a strong metal\u2013support interaction between the Cu-Co nanoparticles and the N-doped carbon matrix, promoting the dispersion of the metal. This study has demonstrated the role of ZIF-derived nitrogen-doped carbon materials in the liquid-phase oxidation and carbonylation of methanol, providing a foundation for subsequent research.<\/jats:p>","DOI":"10.1021\/acsami.6c08512","type":"journal-article","created":{"date-parts":[[2026,9,26]],"date-time":"2026-09-26T19:01:18Z","timestamp":1790449278000},"page":"53292-53301","source":"Crossref","is-referenced-by-count":0,"title":["High Activity of Cu-Co Composite Catalysts Supported on N-Doped Carbon for Dimethyl Carbonate Synthesis via Methanol Oxidative Carbonylation"],"prefix":"10.1021","volume":"18","author":[{"ORCID":"https:\/\/orcid.org\/0009-0002-7519-4041","authenticated-orcid":true,"given":"Xunxun","family":"Li","sequence":"first","affiliation":[{"name":"Zhejiang Institute of Tianjin University , , , ,","place":["Ningbo, Zhejiang, P. R. 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China, 300072"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6808-1244","authenticated-orcid":true,"given":"Hongbo","family":"Yu","sequence":"additional","affiliation":[{"name":"Ningbo University of Technology , , ,","place":["Ningbo, P. R. China, 315211"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-9370-9358","authenticated-orcid":true,"given":"Jing","family":"Lv","sequence":"additional","affiliation":[{"name":"Zhejiang Institute of Tianjin University , , , ,","place":["Ningbo, Zhejiang, P. R. China, 315200"]},{"name":"Tianjin University , , ,","place":["Tianjin, P. R. China, 300072"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2210-0518","authenticated-orcid":true,"given":"Xinbin","family":"Ma","sequence":"additional","affiliation":[{"name":"Tianjin University , , ,","place":["Tianjin, P. R. 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