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Here, we use aberration-corrected analytical scanning transmission electron microscopy to identify the atomic structure and chemistry of a perovskite oxide interface that exhibits different B-site ordering periodicity on the atomic scale. The interface is formed from the 1:1 B-site-ordered double-perovskite Sr2Fe1+xRe1\u2013xO6 and the 1:2 B-site-ordered triple-perovskite Sr3Fe2ReO9. First-principles calculations on the superlattice model with the same modulation of B-site ordering periodicity observed experimentally show that magnetic coupling between Fe and Re atoms at the interface results in characteristics of ferromagnetism, in contrast to the antiferromagnetic nature of the parent phases. The results suggest that tailoring of B-site ordering periodicity for tuning interfacial magnetism at perovskite oxide interfaces can be potentially applied in epitaxial growth of superlattice thin films with magnetically engineered interfaces.<\/jats:p>","DOI":"10.1021\/acsami.6c08939","type":"journal-article","created":{"date-parts":[[2026,9,3]],"date-time":"2026-09-03T16:48:24Z","timestamp":1788454104000},"page":"50054-50063","source":"Crossref","is-referenced-by-count":0,"title":["Perovskite Oxide Interfaces Tailored by Cation Ordering Periodicities: Experimentally Resolved Atomic Structure and Predicted Magnetic Coupling"],"prefix":"10.1021","volume":"18","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-5226-3783","authenticated-orcid":true,"given":"Jie","family":"Ren","sequence":"first","affiliation":[{"name":"City University of Hong Kong , , ,","place":["Kowloon, Hong Kong, China"]},{"name":"City University of Hong Kong Matter Science Research Institute (Futian, Shenzhen) , ,","place":["Shenzhen, China, 518048"]},{"name":"City University of Hong Kong Shenzhen Research Institute , , ,","place":["Shenzhen, China, 518057"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3911-7973","authenticated-orcid":true,"given":"Ping-Luen Baron","family":"Ho","sequence":"additional","affiliation":[{"name":"Imperial College London , , ,","place":["London, U.K., SW7 2AZ"]},{"name":"University of Oxford , , ,","place":["Oxford, U.K., OX1 3QR"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6924-2364","authenticated-orcid":true,"given":"Lei","family":"Jin","sequence":"additional","affiliation":[{"name":"Forschungszentrum J\u00fclich GmbH , , ,","place":["J\u00fclich, Germany, 52425"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1648-142X","authenticated-orcid":true,"given":"Si-Young","family":"Choi","sequence":"additional","affiliation":[{"name":"Pohang University of Science and Technology (POSTECH) , , ,","place":["Pohang, South Korea, 37673"]},{"name":"Institute for Basic Science (IBS) , , ,","place":["Pohang, South Korea, 37673"]},{"name":"Pohang University of Science and Technology (POSTECH) , , ,","place":["Pohang, South Korea, 37673"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Rafal E.","family":"Dunin-Borkowski","sequence":"additional","affiliation":[{"name":"Forschungszentrum J\u00fclich GmbH , , ,","place":["J\u00fclich, Germany, 52425"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3292-5342","authenticated-orcid":true,"given":"Joachim","family":"Mayer","sequence":"additional","affiliation":[{"name":"Forschungszentrum J\u00fclich GmbH , , ,","place":["J\u00fclich, Germany, 52425"]},{"name":"RWTH Aachen University , , ,","place":["Aachen, Germany, 52074"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3601-9320","authenticated-orcid":true,"given":"Sandrine E. M.","family":"Heutz","sequence":"additional","affiliation":[{"name":"Imperial College London , , ,","place":["London, U.K., SW7 2AZ"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Michele Shelly","family":"Conroy","sequence":"additional","affiliation":[{"name":"Imperial College London , , ,","place":["London, U.K., SW7 2AZ"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8796-3146","authenticated-orcid":true,"given":"Shik Chi Edman","family":"Tsang","sequence":"additional","affiliation":[{"name":"University of Oxford , , ,","place":["Oxford, U.K., OX1 3QR"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8990-2198","authenticated-orcid":true,"given":"Xiaoyan","family":"Zhong","sequence":"additional","affiliation":[{"name":"City University of Hong Kong , , ,","place":["Kowloon, Hong Kong, China"]},{"name":"City University of Hong Kong Matter Science Research Institute (Futian, Shenzhen) , ,","place":["Shenzhen, China, 518048"]},{"name":"City University of Hong Kong Shenzhen Research Institute , , ,","place":["Shenzhen, China, 518057"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,2]]},"reference":[{"issue":"7","key":"2026092323291363000_cit1","doi-asserted-by":"publisher","first-page":"734","DOI":"10.3390\/cryst11070734","article-title":"B-Site Cation Ordering in Films, Superlattices, and Layer-by-Layer-Grown Double Perovskites","volume":"11","author":"Ksoll","year":"2021","journal-title":"Crystals"},{"issue":"3","key":"2026092323291363000_cit2","doi-asserted-by":"publisher","first-page":"261","DOI":"10.1557\/mrs.2012.49","article-title":"Control of octahedral connectivity in perovskite oxide heterostructures: An emerging route to multifunctional materials discovery","volume":"37","author":"Rondinelli","year":"2012","journal-title":"MRS Bull."},{"issue":"4","key":"2026092323291363000_cit3","doi-asserted-by":"publisher","first-page":"257","DOI":"10.1038\/s41578-019-0095-2","article-title":"Creating emergent phenomena in oxide superlattices","volume":"4","author":"Ramesh","year":"2019","journal-title":"Nat. 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