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In this work, low-cost NiMnCu-LDH is demonstrated for the first time as a high-performance cathode for AAEs based on Cl\u2013\/CO32\u2013 storage. As paired with the inexpensive hybrid anode of FeO(OH)\/CNT and Bi2O2CO3 in a pouch battery, the AAEs deliver remarkable capacities at 25 and 0 \u00b0C, with \u223c155 and \u223c121 mAh g\u20131 at 300 mA g\u20131, respectively, sufficient to power light-emitting diode devices. Dynamic analysis illustrates mixed kinetics in concert: diffusion-controlled and pseudocapacitive processes. The cost-effectiveness of the AAEs derives from the scalable synthesis of both the NiMnCu-LDH cathode and hybrid anode. The outstanding battery performance is attributed to two-dimensional diffusion channels of LDH facilitating reversible intercalation\/deintercalation of Cl\u2013\/CO32\u2013 within interlayers, along with valence transitions of Ni\/Mn during charge\/discharge cycles. The synergistic effects from mixed anions and the hybrid anode collectively enhance electrochemical performance, in which Cl\u2013 and FeO(OH)\/CNT provide high capacity, while CO32\u2013 and Bi2O2CO3 stabilize cyclicality. These findings highlight the feasibility of the NiMnCu-LDH cathode coupled with the FeO(OH)\/CNT and Bi2O2CO3 anode for AAEs to store Cl\u2013\/CO32\u2013, offering research insights and development opportunities toward sustainable energy storage technologies.<\/jats:p>","DOI":"10.1021\/acsami.6c10960","type":"journal-article","created":{"date-parts":[[2026,9,21]],"date-time":"2026-09-21T06:01:53Z","timestamp":1789970513000},"page":"52543-52554","source":"Crossref","is-referenced-by-count":0,"title":["Aqueous Energy Storage Promoted by Mixed Anions between the NiMnCu-LDH Cathode and Hybrid Anode at 0 \u00b0C"],"prefix":"10.1021","volume":"18","author":[{"given":"Zelin","family":"Wu","sequence":"first","affiliation":[{"name":"Beijing University of Chemical Technology , , ,","place":["Beijing, P. R. 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