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However, the electrochemical performance of MXene phases is often limited by layer restacking, restricted ion accessibility, and insufficient pseudocapacitive activity. Surface-functionalized Ti3C2Tx significantly improves the adsorption properties of MXene phases by adding functional groups that provide reactive sites. In this study, the Ti3C2Tx MXene phases were systematically functionalized with sulphate (SO42\u2013) and phosphate (PO43\u2013) groups through selective acidic treatments using H2SO4\/HF (Tx: -F, -OH, SO42\u2013) and H3PO4\/HF (Tx: -F, -OH, PO43\u2013) solutions. Structural, morphological, and surface chemical analyses confirm the successful incorporation of SO42\u2013 and -PO43\u2013-based functional groups without altering the Ti3C2Tx crystal structure. The SO42\u2013 and PO43\u2013 surface-functionalized MXene phases exhibit markedly enhanced pseudocapacitive behavior, reduced charge-transfer resistance, and improved ion transport kinetics compared with bare Ti3C2Tx MXene. The SO42\u2013-functionalized Ti3C2Tx MXene phases displayed an outstanding specific capacitance of 466 F g\u20131 at 2 A g\u20131 and best thickness-tolerant absorption behavior with a minimum reflection loss of \u201342.6 dB, while the deepest RL value of \u201355.3 dB at 1.5 mm was obtained for Ti3C2Tx MXene.<\/jats:p>","DOI":"10.1021\/acsami.6c11005","type":"journal-article","created":{"date-parts":[[2026,9,4]],"date-time":"2026-09-04T19:02:01Z","timestamp":1788548521000},"page":"50120-50134","source":"Crossref","is-referenced-by-count":1,"title":["Sulphate (\u2013S) and Phosphate (\u2013P) Surface-Functionalized Ti3C2T\n                    <i>x<\/i>\n                    MXene for Enhanced Supercapacitor and Electromagnetic Wave Absorption Performances"],"prefix":"10.1021","volume":"18","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-6171-6307","authenticated-orcid":true,"given":"Yuksel","family":"Akinay","sequence":"first","affiliation":[{"name":"Science Application and Research Center of Van Yuzuncu Yil University , ,","place":["Van, Turkiye, 65080"]},{"name":"Van Yuzuncu Yil University , , ,","place":["Van, Turkiye, 65080"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,4]]},"reference":[{"issue":"10","key":"2026092323291740700_cit1","doi-asserted-by":"publisher","DOI":"10.1002\/SMLL.202412272","article-title":"Bamboo-Inspired Hierarchically Hollow Aerogel MXene Fibers with Ultrafast Ionic Channels and Multiple Electromagnetic Wave Attenuation Routes Toward High-Performance Supercapacitors and Microwave Absorption","volume":"21","author":"Zhang","year":"2025","journal-title":"Small"},{"key":"2026092323291740700_cit2","doi-asserted-by":"publisher","DOI":"10.1016\/J.CARBON.2023.118006","article-title":"Cu1.5Mn1.5O4 Hollow Sphere Decorated Ti3C2Tx MXene for Flexible All-Solid-State Supercapacitor and Electromagnetic Wave Absorber","volume":"209","author":"Zhang","year":"2023","journal-title":"Carbon N. 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