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Four benzoic anhydrides incorporating carbazole or 3,6-di-tert-butylcarbazole donor units, linked to the anhydride acceptor moiety through either para- or ortho-positions, are rationally designed, synthesized, and systematically investigated. Photophysical studies reveal a strong dependence of photophysical properties on the linkage topology. While para-linked derivatives exhibit neither delayed fluorescence nor phosphorescence, ortho-substituted anhydrides display small singlet\u2212triplet energy gaps and consequently show thermally activated delayed fluorescence (TADF), as well as unexpected room-temperature phosphorescence (RTP). Therefore, compounds bearing ortho-linked carbazole donor moieties are successfully employed as triplet-harvesting emitters in sky-blue organic light-emitting diodes (OLEDs), delivering electroluminescence maxima at 475 and 481 nm, maximum external quantum efficiencies of up to 21.0%, high luminance exceeding 62 000 cd\/m2, and low efficiency roll-off. These results demonstrate that the formation of anhydrides from donor-substituted aromatic acids represents a versatile and effective design strategy for highly emissive TADF\/RTP materials and provides a promising platform for the development of efficient multicolor OLED emitters through rational molecular engineering.<\/jats:p>","DOI":"10.1021\/acsami.6c11053","type":"journal-article","created":{"date-parts":[[2026,8,19]],"date-time":"2026-08-19T00:02:09Z","timestamp":1787097729000},"page":"51286-51298","source":"Crossref","is-referenced-by-count":0,"title":["Carbazolyl-Substituted Benzoic Anhydrides as Efficient Triplet Harvesters for High-Brightness Blue Organic Light-Emitting Diodes"],"prefix":"10.1021","volume":"18","author":[{"given":"Myroslava","family":"Aksionova","sequence":"first","affiliation":[{"name":"Ivan Franko National University of Lviv , , Kyryla i Mefodiya 6 , ,","place":["Lviv, Ukraine, 79005"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Khrystyna","family":"Ivaniuk","sequence":"additional","affiliation":[{"name":"Lviv Polytechnic National University , , Sviatoho Yura sq. 1 , ,","place":["Lviv, Ukraine, 79013"]},{"name":"Polish Academy of Sciences , , Kasprzaka 44\/52 , ,","place":["Warsaw, Poland, 01-224"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7086-9703","authenticated-orcid":true,"given":"Roman","family":"Lytvyn","sequence":"additional","affiliation":[{"name":"Ivan Franko National University of Lviv , , Kyryla i Mefodiya 6 , ,","place":["Lviv, Ukraine, 79005"]},{"name":"Polish Academy of Sciences , , Kasprzaka 44\/52 , ,","place":["Warsaw, Poland, 01-224"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0757-6059","authenticated-orcid":true,"given":"Stepan","family":"Kutsiy","sequence":"additional","affiliation":[{"name":"Lviv Polytechnic National University , , Sviatoho Yura sq. 1 , ,","place":["Lviv, Ukraine, 79013"]},{"name":"Polish Academy of Sciences , , Kasprzaka 44\/52 , ,","place":["Warsaw, Poland, 01-224"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Oskar","family":"Kaszubowski","sequence":"additional","affiliation":[{"name":"University of Wroc\u0142aw , , F. Joliot-Curie 14 , ,","place":["Wroc\u0142aw, Poland, 50-383"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1060-0459","authenticated-orcid":true,"given":"Vasyl","family":"Kinzhybalo","sequence":"additional","affiliation":[{"name":"Institute of Low Temperature and Structure Research, Polish Academy of Sciences , Ok\u00f3lna 2 , ,","place":["Wroc\u0142aw, Poland, 50-422"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Asta","family":"Dabulien\u0117","sequence":"additional","affiliation":[{"name":"Kaunas University of Technology , , Barsausko 59 , ,","place":["Kaunas, Lithuania, LT-51423"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3526-2679","authenticated-orcid":true,"given":"Dmytro","family":"Volyniuk","sequence":"additional","affiliation":[{"name":"Kaunas University of Technology , , Barsausko 59 , ,","place":["Kaunas, Lithuania, LT-51423"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8146-9529","authenticated-orcid":true,"given":"Mykola D.","family":"Obushak","sequence":"additional","affiliation":[{"name":"Ivan Franko National University of Lviv , , Kyryla i Mefodiya 6 , ,","place":["Lviv, Ukraine, 79005"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4408-9727","authenticated-orcid":true,"given":"Juozas Vidas","family":"Grazulevicius","sequence":"additional","affiliation":[{"name":"Kaunas University of Technology , , Barsausko 59 , ,","place":["Kaunas, Lithuania, LT-51423"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4543-2785","authenticated-orcid":true,"given":"Mykhaylo A.","family":"Potopnyk","sequence":"additional","affiliation":[{"name":"Ivan Franko National University of Lviv , , Kyryla i Mefodiya 6 , ,","place":["Lviv, Ukraine, 79005"]},{"name":"Polish Academy of Sciences , , Kasprzaka 44\/52 , ,","place":["Warsaw, Poland, 01-224"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,18]]},"reference":[{"issue":"24","key":"2026092306072855400_cit1","doi-asserted-by":"publisher","first-page":"13736","DOI":"10.1021\/acs.chemrev.3c00755","article-title":"The Golden Age of Thermally Activated Delayed Fluorescence Materials: Design and Exploitation","volume":"124","author":"Dos Santos","year":"2024","journal-title":"Chem. 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