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However, the Jahn\u2013Teller effect results in unfavorable structural distortion and capacity fade. Herein, a Ti4+ and Br\u2013 codoping strategy to enhance structural stability and electronic\/ionic conductivity is proposed. Ti4+ substitutes for Fe\/Mn sites, acting as a donor dopant with strong Ti\u2013O bond. Br\u2013 widens the ion channel with the larger ionic radius. The results show that it leads to a 60-fold surge in carrier density, a 9-fold improvement in electronic conductivity, and increase the ionic mobility to 2 \u00d7 10\u201311 cm2 s\u20131 (nearly 20-fold). Besides, ex-situ XRD analysis reveals a nearly zero structural strain (0.2%) during cycling. Ex-situ XPS analysis reveals the proportions of V5+ and Mn4+ increase significantly after constant-voltage charging at 4.4 V. Meanwhile, the V2+\/V3+ redox couple is activated within 1.0\u20131.8 V. The optimized Na4Fe0.4Mn0.4Ti0.2V(PO4)2.9Br0.3 cathode demonstrates a remarkable discharge capacity of 183.8 mAh g\u20131 at 0.1C within 1.0\u20134.4 V and even 115.5 mAh g\u20131 at 5C with a retention of 82.4% after 5000 cycles. Importantly, its sodium-ion storage properties have been successfully validated under high-areal-loading conditions, which indicates it could be a promising cathode.<\/jats:p>","DOI":"10.1021\/acsami.6c11782","type":"journal-article","created":{"date-parts":[[2026,9,24]],"date-time":"2026-09-24T18:02:03Z","timestamp":1790272923000},"page":"53338-53352","source":"Crossref","is-referenced-by-count":0,"title":["An Effective Cation\u2013Anion Codoping Strategy for Superior Stability and High-Performance of Na4Fe0.5Mn0.5V(PO4)3 Cathode"],"prefix":"10.1021","volume":"18","author":[{"given":"Zhuohui","family":"Sun","sequence":"first","affiliation":[{"name":"Xi'an Jiaotong University , , ,","place":["Xi'an, China, 710049"]},{"name":"Xi'an Jiaotong University , , ,","place":["Xi'an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hongwei","family":"Zhang","sequence":"additional","affiliation":[{"name":"Xi'an Jiaotong University , , ,","place":["Xi'an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yilong","family":"Jia","sequence":"additional","affiliation":[{"name":"Xi'an Jiaotong University , , ,","place":["Xi'an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Li","family":"Cao","sequence":"additional","affiliation":[{"name":"Xi'an Jiaotong University , , ,","place":["Xi'an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0003-0742-8480","authenticated-orcid":true,"given":"Youlong","family":"Xu","sequence":"additional","affiliation":[{"name":"Xi'an Jiaotong University , , ,","place":["Xi'an, China, 710049"]},{"name":"Xi'an Jiaotong University , , ,","place":["Xi'an, China, 710049"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,24]]},"reference":[{"key":"2026100711081565500_cit1","doi-asserted-by":"publisher","DOI":"10.1016\/j.est.2025.116511","article-title":"Advancing energy storage: The future trajectory of lithium-ion battery technologies","volume":"120","author":"Hasan","year":"2025","journal-title":"J. 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