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Poly(vinylidene fluoride) (PVDF), prized for its exceptional chemical and mechanical stability, faces a long-standing performance trade-off, as its inherent hydrophobicity causes severe biofouling, while chlorine regeneration for biofilm removal degrades surface-grafted antibacterial functional layers. Herein, we report a high-performance chlorine-rechargeable N-halamine antibacterial membrane (denoted as PPVDF-O-TP-Cl, a PEG-blended PVDF grafted with chlorinated TMP moieties) fabricated via an integrated \u201cpassive defense-active attack\u201d strategy, featuring covalent surface anchoring of sterically hindered 2,2,6,6-tetramethylpiperidine (TMP-OH) onto PVDF backbones through ester linkages. The membrane achieved robust broad-spectrum antibacterial efficacy, delivering a 6.1-log reduction against Gram-negative E. coli and a 5.5-log reduction against Gram-positive S. aureus within 30 min, a flux recovery ratio exceeding 90.0%, and retained over 99% antibacterial activity after 10 chlorination-regeneration cycles. Notably, TMP\u2019s bulky methyl groups sterically shield vulnerable ester bonds from hydrolytic and oxidative degradation, while PEG hydration layers and N-halamine moieties synergistically mitigate the interfacial kinetic imbalance plaguing traditional membranes. This work provides a versatile strategy for designing durable rechargeable anti-biofouling membranes, with future investigations warranted into their long-term performance in complex real wastewater matrices and scalable fabrication.<\/jats:p>","DOI":"10.1021\/acsami.6c12016","type":"journal-article","created":{"date-parts":[[2026,9,1]],"date-time":"2026-09-01T22:00:48Z","timestamp":1788300048000},"page":"47436-47449","source":"Crossref","is-referenced-by-count":0,"title":["Ester Bond-Anchored TMP Moieties for Durable and Rechargeable Anti-biofouling PVDF Membranes"],"prefix":"10.1021","volume":"18","author":[{"given":"Hao","family":"Yang","sequence":"first","affiliation":[{"name":"Nanjing University of Posts & Telecommunications , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Feifan","family":"Shi","sequence":"additional","affiliation":[{"name":"Nanjing University of Posts & Telecommunications , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yihang","family":"Li","sequence":"additional","affiliation":[{"name":"Nanjing University of Posts & Telecommunications , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Rujing","family":"Shen","sequence":"additional","affiliation":[{"name":"Nanjing University of Posts & Telecommunications , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wei","family":"Wei","sequence":"additional","affiliation":[{"name":"Nanjing University of Posts & Telecommunications , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1631-7072","authenticated-orcid":true,"given":"Ang","family":"Wei","sequence":"additional","affiliation":[{"name":"Nanjing University of Posts & Telecommunications , , ,","place":["Nanjing, China, 210023"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,27]]},"reference":[{"key":"2026091612073274800_cit1","doi-asserted-by":"publisher","DOI":"10.1016\/j.seppur.2024.130140","article-title":"Unlocking the potential of graphene oxide membranes: Microstructural tuning through metal\u2013organic frameworks for water treatment progress","volume":"357","author":"Qian","year":"2025","journal-title":"Sep. 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