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To counteract this, rigid, nonplanar building blocks with aliphatic C\u2013H units, contorted Tr\u00f6ger\u2019s base (TB) units, are integrated into microporous organic polymers (MOPs), where micropores enable rapid physisorption, tertiary nitrogen sites allow stable chemisorption, and the aliphatic C\u2013H units within these scaffolds restrict conjugation and donate electrons to benzene rings, further promoting continuous NOx adsorption. Among the polymers, triptycene-based TB (Trip-TB, 1011 m2 g\u20131, 3.36 mmol g\u20131) and tetraphenyladamantane-based TB (TAPA-TB, 826 m2 g\u20131, 3.32 mmol g\u20131) outperform the triphenylbenzene analog (TAPB-TB, 926 m2 g\u20131, 2.99 mmol g\u20131). With only 3 wt% Trip-TB, NOx release is reduced by 70.2 % in titration tests, and the methyl violet color-change time extends 3.15-fold. This enhancement is attributed to the conjugation-interrupting and electron-donating effects of the aliphatic cores to the benzene rings. Characterization and calculations further elucidate the adsorption mechanism. Collectively, these findings establish a cooperative physicochemical mechanism for efficient NOx capture and provide a rational blueprint for adsorbent design.<\/jats:p>","DOI":"10.1021\/acsami.6c12272","type":"journal-article","created":{"date-parts":[[2026,8,10]],"date-time":"2026-08-10T04:01:49Z","timestamp":1786334509000},"page":"44497-44506","source":"Crossref","is-referenced-by-count":0,"title":["Three-Dimensional Nonconjugated Microporous Organic Polymers Based on Tr\u00f6ger\u2019s Base: Integrating Physical Confinement and Chemisorption for Enhanced NO\n                    <i>x<\/i>\n                    Capture"],"prefix":"10.1021","volume":"18","author":[{"given":"Huimin","family":"Chen","sequence":"first","affiliation":[{"name":"Nanjing University of Science and Technology , , ,","place":["Nanjing, China, 210094"]},{"name":"Key Laboratory of Special Energy Materials, Ministry of Education , ,","place":["Nanjing, China, 210094"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin","family":"Li","sequence":"additional","affiliation":[{"name":"Nanjing University of Science and Technology , , ,","place":["Nanjing, China, 210094"]},{"name":"Key Laboratory of Special Energy Materials, Ministry of Education , ,","place":["Nanjing, China, 210094"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wenjiang","family":"Li","sequence":"additional","affiliation":[{"name":"Nanjing University of Science and Technology , , ,","place":["Nanjing, China, 210094"]},{"name":"Key Laboratory of Special Energy Materials, Ministry of Education , ,","place":["Nanjing, China, 210094"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lihong","family":"Ran","sequence":"additional","affiliation":[{"name":"Nanjing University of Science and Technology , , ,","place":["Nanjing, China, 210094"]},{"name":"Key Laboratory of Special Energy Materials, Ministry of Education , ,","place":["Nanjing, China, 210094"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chenguang","family":"Li","sequence":"additional","affiliation":[{"name":"Nanjing University of Science and Technology , , ,","place":["Nanjing, China, 210094"]},{"name":"Key Laboratory of Special Energy Materials, Ministry of Education , ,","place":["Nanjing, China, 210094"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Dabin","family":"Liu","sequence":"additional","affiliation":[{"name":"Nanjing University of Science and Technology , , ,","place":["Nanjing, China, 210094"]},{"name":"Key Laboratory of Special Energy Materials, Ministry of Education , ,","place":["Nanjing, China, 210094"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3729-1828","authenticated-orcid":true,"given":"Binbin","family":"Wang","sequence":"additional","affiliation":[{"name":"Nanjing University of Science and Technology , , ,","place":["Nanjing, China, 210094"]},{"name":"Key Laboratory of Special Energy Materials, Ministry of Education , ,","place":["Nanjing, China, 210094"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,9]]},"reference":[{"key":"2026081907191527100_cit1","doi-asserted-by":"publisher","first-page":"133","DOI":"10.1016\/j.coche.2016.09.004","article-title":"Impact of nitrogen oxides on the environment and human health: Mn-based materials for the NOx abatement","volume":"13","author":"Boningari","year":"2016","journal-title":"Curr. 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