{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,24]],"date-time":"2026-10-24T09:29:09Z","timestamp":1792834149935,"version":"4.5.0"},"reference-count":53,"publisher":"American Chemical Society (ACS)","issue":"40","license":[{"start":{"date-parts":[[2026,10,1]],"date-time":"2026-10-01T00:00:00Z","timestamp":1790812800000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-029"},{"start":{"date-parts":[[2026,10,1]],"date-time":"2026-10-01T00:00:00Z","timestamp":1790812800000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-037"},{"start":{"date-parts":[[2026,10,1]],"date-time":"2026-10-01T00:00:00Z","timestamp":1790812800000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-045"}],"funder":[{"DOI":"10.13039\/501100003645","name":"National Cancer Center","doi-asserted-by":"publisher","award":["NCC2020PY12"],"award-info":[{"award-number":["NCC2020PY12"]}],"id":[{"id":"10.13039\/501100003645","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,10,14]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>The efficient development of high-performance complex biological sample-compatible fluorescent molecularly imprinted polymers (MIPs) and their portable sensors is highly important for their real-world applications but remains challenging. Herein, we report on the efficient synthesis of hydrophilic hairy dual signal-responsive ratiometric fluorescent MIP microspheres and their smartphone-assisted highly sensitive and precise visual detection of 2,4-dichlorophenoxyacetic acid (2,4-D) in the undiluted pure milks. Core-shell-corona-structured 2,4-D-MIP particles with both green and red fluorescent species-labeling and polyethylene glycol brushes were readily synthesized via the newly developed one-pot surface-initiated activator-regenerated by electron transfer atom transfer radical polymerization (ATRP) with tris[2-(dimethylamino)ethyl]amine as both the ligand and the reducing agent for Cu(II) catalyst. This synthetic strategy could not only afford largely enhanced polymerization rate but also lead to fluorescent 2,4-D-MIP particles with obviously enhanced fluorescence responses toward 2,4-D compared with those prepared via the previously developed one-pot surface-initiated ATRP methods. Such hydrophilic dual fluorescent 2,4-D-MIP showed remarkable photostability, reusability, and long-term storage stability as well as strong 2,4-D selectivity and simultaneous large green fluorescence enhancement and red fluorescence quenching toward 2,4-D in pure milk samples, which make them promising complex biological sample-compatible chemosensors for visually detecting 2,4-D with good recoveries (98.0\u2013104.0%) and high accuracy (\u22644.0%). Notably, their obvious dual-signal responsivity imparted them with significantly enhanced optosensing sensitivity, with their limit of detection (=0.025 \u03bcM) being almost five times lower than that of our previously reported hydrophilic hairy single signal-responsive ratiometric fluorescent 2,4-D-MIPs. Finally, a smartphone-integrated portable MIP optosensor was developed for precise and selective visual 2,4-D detection in pure milks. This study opens new access for efficient development of high-performance MIP optosensors highly promising in on-site detection of complex biological samples.<\/jats:p>","DOI":"10.1021\/acsami.6c13576","type":"journal-article","created":{"date-parts":[[2026,10,1]],"date-time":"2026-10-01T08:01:35Z","timestamp":1790841695000},"page":"55433-55445","source":"Crossref","is-referenced-by-count":1,"title":["Hydrophilic Hairy Dual Signal-Responsive Ratiometric Fluorescent Molecularly Imprinted Polymer Microspheres for Smartphone-Assisted Visual Herbicide Detection in the Undiluted Milks"],"prefix":"10.1021","volume":"18","author":[{"given":"Shakir","family":"Ullah","sequence":"first","affiliation":[{"name":"Nankai University , , ,","place":["Tianjin, China, 300071"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yanyan","family":"Mu","sequence":"additional","affiliation":[{"name":"Nankai University , , ,","place":["Tianjin, China, 300071"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yifan","family":"Zhang","sequence":"additional","affiliation":[{"name":"Nankai University , , ,","place":["Tianjin, China, 300071"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8430-691X","authenticated-orcid":true,"given":"Huiqi","family":"Zhang","sequence":"additional","affiliation":[{"name":"Nankai University , , ,","place":["Tianjin, China, 300071"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,10,1]]},"reference":[{"key":"2026101408072378600_cit1","doi-asserted-by":"publisher","DOI":"10.1016\/j.ecoenv.2025.118715","article-title":"Phenoxycarboxylic Acid Herbicides in Environment: Recent Updates on Pretreatment and Analysis Methods","volume":"302","author":"Ren","year":"2025","journal-title":"Ecotoxicol. 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