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Here, we present hierarchically structured gold-leaf\/WPU\/TPU fibers prepared through a twisted coating route. With waterborne polyurethane (WPU) used as the adhesive interlayer, a strip of nano-gold leaf was transferred onto the surface of the pretwisted TPU fiber, and release of the stored twist converted the metal layer into a helical conductive path accompanied by surface buckling. The helical turn density governed both the wrinkle morphology and the strain-dependent resistance. After WPU encapsulation, the helical gold-leaf\/WPU\/TPU fibers (HGLWTFs) with a helical turn density of 0.5 turn\/cm exhibited a stable and monotonic resistive response, with a gauge factor (GF) of 25.7 over 0\u2013100% strain, response\/recovery times of 192\/243 ms, stable performance over 1000 stretching cycles at 30% strain, and an electrical conductivity of 5.70 \u00d7 106 S\/m. The HGLWTFs were further thermoformed into superelastic electrodes, retaining an electrical conductivity of 4.62 \u00d7 106 S\/m and reaching a Q value of 363.6 at 2000% strain. The DHGLWTF capacitive sensor exhibited a linear strain response with R2 = 0.997 and response\/recovery times of 46\/72 ms and detectable capacitance changes during finger approach. A smart textile glove assembled with HGLWTFs was further used for remote manipulation of a robotic hand. These results highlight the potential of hierarchical gold-leaf fiber conductors for wearable sensing, stretchable electrodes, and human-machine interfaces.<\/jats:p>","DOI":"10.1021\/acsami.6c13829","type":"journal-article","created":{"date-parts":[[2026,9,17]],"date-time":"2026-09-17T23:01:15Z","timestamp":1789686075000},"page":"52761-52773","source":"Crossref","is-referenced-by-count":0,"title":["Hierarchically Helical and Buckled Gold Leaf on TPU Fibers for Superelastic Electrodes and Multifunctional Sensors"],"prefix":"10.1021","volume":"18","author":[{"given":"Yihao","family":"Zhou","sequence":"first","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]},{"name":"Engineering Research Center of Optical Instruments and Systems , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wei","family":"Kang","sequence":"additional","affiliation":[{"name":"Shanghai Aerospace Control Technology Institute , ,","place":["Shanghai, China, 201109"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xufang","family":"Fan","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]},{"name":"Engineering Research Center of Optical Instruments and Systems , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Kaixin","family":"Li","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]},{"name":"Engineering Research Center of Optical Instruments and Systems , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shangbi","family":"Chen","sequence":"additional","affiliation":[{"name":"Shanghai Aerospace Control Technology Institute , ,","place":["Shanghai, China, 201109"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9874-7705","authenticated-orcid":true,"given":"Bin","family":"Sheng","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]},{"name":"Engineering Research Center of Optical Instruments and Systems , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,17]]},"reference":[{"issue":"42","key":"2026093002065681500_cit1","doi-asserted-by":"publisher","DOI":"10.1002\/adfm.202104686","article-title":"Recent Progress in Essential Functions of Soft Electronic Skin","volume":"31","author":"Chen","year":"2021","journal-title":"Adv. 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