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Transition metal selenides (TMSs) offer favorable electrical conductivity, inexpensive constituents, and adjustable electronic configurations; however, their inherent catalytic activity is still insufficient. In this study, nanorod-like Fe\/Co co-doped NiSe (Fe,Co\u2013NiSe) was prepared by hydrothermally forming NiSe and subsequently introducing Fe and Co through a simple soaking treatment. The simultaneous incorporation of Fe and Co effectively tunes the electronic structure of NiSe. Raman measurements performed in situ show that introducing Fe\/Co favors the generation of NiOOH-type oxyhydroxide species, thereby enhancing OER activity. 18O-labeling differential electrochemical mass spectrometry confirms that Fe,Co\u2013NiSe follows the conventional adsorbate evolution mechanism. Density functional theory (DFT) analysis further indicates that Fe-induced electronic redistribution at Co sites raises the Co d-band position and reduces the Gibbs energy required for the kinetically limiting *O \u2192 *OOH conversion. Consequently, under alkaline conditions, Fe,Co\u2013NiSe reaches 10 mA cm\u20132 at an overpotential of 229 mV and sustains 50 mA cm\u20132 for 300 h. When employed as the anodic electrode in an anion exchange membrane (AEM) water electrolyzer coupled with Pt\/C, this electrolyzer delivers 1 A cm\u20132 while registering a cell voltage of 1.84 V.<\/jats:p>","DOI":"10.1021\/acsami.6c14042","type":"journal-article","created":{"date-parts":[[2026,9,29]],"date-time":"2026-09-29T09:02:45Z","timestamp":1790672565000},"page":"54908-54918","source":"Crossref","is-referenced-by-count":0,"title":["Efficient and Stable Alkaline Oxygen Evolution on Fe\/Co Co-Doped NiSe"],"prefix":"10.1021","volume":"18","author":[{"given":"Chao","family":"Wang","sequence":"first","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0006-9971-8267","authenticated-orcid":true,"given":"Qing","family":"Zhang","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0005-2473-2788","authenticated-orcid":true,"given":"Cong","family":"Liu","sequence":"additional","affiliation":[{"name":"East China University of Science and Technology , , ,","place":["Shanghai, China, 200237"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Haishun","family":"Jiang","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3870-624X","authenticated-orcid":true,"given":"Wan","family":"Zhou","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1371-4817","authenticated-orcid":true,"given":"Muhammad","family":"Nadeem","sequence":"additional","affiliation":[{"name":"AIIM Building Innovation Campus, University of Wollongong , ,","place":["Wollongong, Australia, 2525"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qiaoliang","family":"Bao","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6543-5529","authenticated-orcid":true,"given":"Yoshio","family":"Bando","sequence":"additional","affiliation":[{"name":"AIIM Building Innovation Campus, University of Wollongong , ,","place":["Wollongong, Australia, 2525"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ding","family":"Yuan","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2549-1400","authenticated-orcid":true,"given":"Yuhai","family":"Dou","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,29]]},"reference":[{"issue":"9","key":"2026101406073958000_cit1","doi-asserted-by":"publisher","first-page":"3170","DOI":"10.1039\/d2cs00368f","article-title":"Dinuclear metal synergistic catalysis for energy conversion","volume":"52","author":"Zhong","year":"2023","journal-title":"Chem. 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