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In this study, a large-scale polymer-derived silicon boron carbonitride (SiBCN)-reinforced BN hybrid aerogel (SiBCN\/BN) was fabricated via impregnation, solvothermal treatment, and pyrolysis; critically, the SiBCN aerogels construct a mesoporous network within the macropores of the BN nanoribbon skeleton. The density (0.073\u20130.236 g\u00b7cm\u20133) and the micromorphology of the SiBCN\/BN hybrid aerogels can be tuned by adjusting the SiBCN loading. The hierarchical pore structure endows the SiBCN\/BN aerogel with low thermal conductivity at room temperature (0.042 W\u00b7m\u20131\u00b7K\u20131) and at high temperature (0.061 W m\u20131 K\u20131 @ 800 \u00b0C and 0.080 W m\u20131 K\u20131 @ 1000 \u00b0C). Notably, the SiBCN\/BN hybrid aerogel exhibits enhanced compressive strength (1.36 MPa, 405-fold higher than that of the BN aerogel) and improved ablation resistance (only 1% linear shrinkage after 1000 \u00b0C ablation). These superior properties are attributable to the reinforcement and protective effects imparted by the SiBCN phase. Furthermore, the SiBCN\/BN hybrid aerogel shows super-hydrophobicity with a water contact angle up to 150.6\u00b0, endowing it with self-cleaning and moisture-resistant properties. The synergistic enhancement in mechanical strength and thermal stability makes the SiBCN\/BN hybrid aerogel an exceptional choice for lightweight thermal insulation, expanding its practical utility and paving the way for next-generation multifunctional, robust, and durable aerogel systems.<\/jats:p>","DOI":"10.1021\/acsami.6c14990","type":"journal-article","created":{"date-parts":[[2026,9,26]],"date-time":"2026-09-26T10:01:28Z","timestamp":1790416888000},"page":"54049-54061","source":"Crossref","is-referenced-by-count":0,"title":["Lightweight and Super-Hydrophobic SiBCN-Reinforced BN Nanoribbon Aerogel for High-Temperature Thermal Insulation"],"prefix":"10.1021","volume":"18","author":[{"given":"Mingxin","family":"Lu","sequence":"first","affiliation":[{"name":"Tianjin University , , ,","place":["Tianjin, China, 300350"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wenxia","family":"Zhu","sequence":"additional","affiliation":[{"name":"Tianjin University , , ,","place":["Tianjin, China, 300350"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8553-9758","authenticated-orcid":true,"given":"Dong","family":"Su","sequence":"additional","affiliation":[{"name":"Tianjin University , , ,","place":["Tianjin, China, 300350"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,26]]},"reference":[{"key":"2026100915082524100_cit1","doi-asserted-by":"publisher","first-page":"341","DOI":"10.1016\/j.actaastro.2020.06.047","article-title":"Thermal protection systems for space vehicles: A review on technology development, current challenges and future prospects","volume":"176","author":"Uyanna","year":"2020","journal-title":"Acta Astronaut."},{"issue":"2","key":"2026100915082524100_cit2","doi-asserted-by":"publisher","first-page":"81","DOI":"10.1038\/s41578-022-00496-z","article-title":"Materials for extreme environments","volume":"8","author":"Eswarappa Prameela","year":"2022","journal-title":"Nat. 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