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Herein, we report a pair of chiral lanthanide complex isomers (GXU-1\/2) with a full-width at half-maximum (FWHM) of only 8 nm and the highest LY constructed via the synergism of aggregation-enhanced antenna effect from aggregation-induced emission luminogens (AIEgens) and secondary antenna effect from rigid auxiliary ligands. Two pairs of chiral lanthanide complex isomers GXU-1\/2 and GXU-3\/4 both showed significant aggregation-enhanced antenna effects, exhibiting bright lysosome optical imaging effects. This dual-antenna strategy endows the materials with efficient energy transfer to Eu(III), confirmed by femtosecond transient absorption spectroscopy. GXU-1 achieves an ultrahigh LY of 70,199 photons MeV\u20131, an extremely low detection limit of 52.52 nGy\u00b7s\u20131 (over 105-fold lower than clinical diagnostic standard (5.5 \u03bcGy\/s)), and an ultranarrow full-width at half-maximum of only 8 nm, with red emission purity closely matching the BT.2020 standard. This work offers a general route for high-performance lanthanide X-ray scintillators.<\/jats:p>","DOI":"10.1021\/acsami.6c16202","type":"journal-article","created":{"date-parts":[[2026,9,24]],"date-time":"2026-09-24T10:01:55Z","timestamp":1790244115000},"page":"53684-53697","source":"Crossref","is-referenced-by-count":0,"title":["Chiral Lanthanide Complex Isomers Enable Ultra-High-Brightness Narrowband X-Ray Scintillation and Lysosome Optical Imaging via Aggregation and Dual-Antenna Effects"],"prefix":"10.1021","volume":"18","author":[{"given":"Ying","family":"Gong","sequence":"first","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"De-Xin","family":"Chen","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fan","family":"Yang","sequence":"additional","affiliation":[{"name":"Guangxi Normal University , , ,","place":["Guilin, P. R. China, 541004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wen-Kang","family":"Jiang","sequence":"additional","affiliation":[{"name":"Guangxi Normal University , , ,","place":["Guilin, P. R. China, 541004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3664-4022","authenticated-orcid":true,"given":"Hai-Ling","family":"Wang","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Meng-Juan","family":"Tang","sequence":"additional","affiliation":[{"name":"Guangxi Normal University , , ,","place":["Guilin, P. R. China, 541004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ru-Yan","family":"Li","sequence":"additional","affiliation":[{"name":"Guangxi University , , ,","place":["Nanning, P. R. China, 530004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7435-0140","authenticated-orcid":true,"given":"Fu-Pei","family":"Liang","sequence":"additional","affiliation":[{"name":"Guangxi Normal University , , ,","place":["Guilin, P. R. China, 541004"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1759-3714","authenticated-orcid":true,"given":"Hua-Hong","family":"Zou","sequence":"additional","affiliation":[{"name":"Guangxi Normal University , , ,","place":["Guilin, P. R. 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