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Differential electrochemical mass spectrometry and comparative OCP measurements identify hydrogen evolution and oxygen-associated reoxidation as self-discharge pathways of the dianion, motivating operation within a restricted potential window. XPS and EDX measurements support Na-ion coordination to reduced carbonyls as the principal charge-compensation mechanism. In a symmetric PTCDI cell, the selected redox couple retains 88% of its capacity after more than 19,000 cycles with near-unity coulombic efficiency. At nominal charge times of 60 and 2 s, the electrode retains 86 and 41% of its theoretical capacity, respectively, demonstrating ultrafast kinetics without sacrificing durability. These results establish redox-selective control as a design strategy for aqueous carbonyl electrodes whose deeper reduction approaches the stability limit of water.<\/jats:p>","DOI":"10.1021\/acsami.6c16356","type":"journal-article","created":{"date-parts":[[2026,10,7]],"date-time":"2026-10-07T19:02:10Z","timestamp":1791399730000},"source":"Crossref","is-referenced-by-count":0,"title":["Redox-Selective Control of Perylene Diimide Enables Fast, Durable Aqueous Sodium-Ion Storage"],"prefix":"10.1021","author":[{"ORCID":"https:\/\/orcid.org\/0009-0002-6062-5283","authenticated-orcid":true,"given":"Sebastian","family":"Liebl","sequence":"first","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Christoph","family":"Griesser","sequence":"additional","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8196-0761","authenticated-orcid":true,"given":"Sergio","family":"D\u00edaz-Coello","sequence":"additional","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0006-2286-7205","authenticated-orcid":true,"given":"Toni","family":"Moser","sequence":"additional","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0005-0246-0507","authenticated-orcid":true,"given":"Philip","family":"Eck","sequence":"additional","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Daniel","family":"Werner","sequence":"additional","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8225-3110","authenticated-orcid":true,"given":"Julia","family":"Kunze-Liebh\u00e4user","sequence":"additional","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6281-5243","authenticated-orcid":true,"given":"Engelbert","family":"Portenkirchner","sequence":"additional","affiliation":[{"name":"University of Innsbruck , , Innrain 52c , ,","place":["Innsbruck, Austria, 6020"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,10,7]]},"reference":[{"issue":"1","key":"2026100715015987700_cit1","doi-asserted-by":"publisher","first-page":"19","DOI":"10.1038\/nchem.2085","article-title":"Towards Greener and More Sustainable Batteries for Electrical Energy Storage","volume":"7","author":"Larcher","year":"2014","journal-title":"Nat. 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