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However, inherent incompatibilities between these catalytic systems have impeded progress in this area, particularly regarding their efficient coimmobilization within a single carrier. Herein, we report a general Pickering emulsion-driven interfacial coassembly strategy to construct modular micro\/nanoreactors that enable the precise spatial integration of metal nanoparticles and multiple enzymes within a porous crystalline framework, including diverse metal\u2013organic frameworks and covalent organic frameworks. These compartmentalized reactors orchestrate efficient chemoenzymatic one-pot reactions, as demonstrated by the dynamic kinetic resolution of racemic amines via synergistic Pd\/enzyme catalysis. Furthermore, this architecture drives effective photoenzymatic cascades and exhibits robust utility in degrading pollutants under demanding conditions. By overcoming limitations inherent to conventional strategies, such as restricted carrier compatibility, insufficient active site exposure, and constrained mass transfer, this work provides a universal solution for integrating otherwise incompatible catalytic reactions.<\/jats:p>","DOI":"10.1021\/acsnano.6c07882","type":"journal-article","created":{"date-parts":[[2026,9,7]],"date-time":"2026-09-07T11:01:52Z","timestamp":1788778912000},"page":"25420-25429","source":"Crossref","is-referenced-by-count":1,"title":["Bridging Catalytic\nWorlds: A Coassembly Platform for\nUnified Chemoenzymatic Cascades"],"prefix":"10.1021","volume":"20","author":[{"given":"Yanhua","family":"Zhao","sequence":"first","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]},{"name":"Northwestern Polytechnical University , , 127 West Youyi Road , ,","place":["Xi\u2019an, China, 710072"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xingyue","family":"Ji","sequence":"additional","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Na","family":"Jin","sequence":"additional","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Kexin","family":"Li","sequence":"additional","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yuqing","family":"Niu","sequence":"additional","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Cheng","family":"Chen","sequence":"additional","affiliation":[{"name":"Xiamen University , , Xiang\u2019an South Road , , ,","place":["Xiamen, Fujian, China, 361102"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yun","family":"Fan","sequence":"additional","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5318-4267","authenticated-orcid":true,"given":"Fengwei","family":"Huo","sequence":"additional","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]},{"name":"Xiamen University , , Xiang\u2019an South Road , , ,","place":["Xiamen, Fujian, China, 361102"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-0904-6008","authenticated-orcid":true,"given":"Weina","family":"Zhang","sequence":"additional","affiliation":[{"name":"Nanjing Tech University (NanjingTech) , , 30 South Puzhu Road , ,","place":["Nanjing, China, 211816"]},{"name":"Northwestern Polytechnical University , , 127 West Youyi Road , ,","place":["Xi\u2019an, China, 710072"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,7]]},"reference":[{"issue":"6562","key":"2026092210072114800_cit1","doi-asserted-by":"publisher","first-page":"1523","DOI":"10.1126\/science.abh4049","article-title":"Cell-free chemoenzymatic starch synthesis from carbon dioxide","volume":"373","author":"Cai","year":"2021","journal-title":"Science"},{"issue":"10","key":"2026092210072114800_cit2","doi-asserted-by":"publisher","first-page":"1275","DOI":"10.1038\/s44160-024-00591-9","article-title":"Chemoenzymatic\nsynthesis of macrocycles via dynamic kinetic resolution of secondary\nalcohols","volume":"3","author":"Guerrero-Morales","year":"2024","journal-title":"Nat. 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