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Here we report a strategy to overcome this limitation using 1,4-disubstituted benzene-based molecular rotors engineered for maximal rotational freedom. These motifs self-assemble into loosely packed architectures that simultaneously suppress intermolecular quenching and steric strain, thereby unlocking an aggregated twisted intramolecular charge transfer (A-TICT) state absent in tightly stacked analogues. Through femtosecond transient absorption and time-resolved circularly polarized luminescence (CPL) spectroscopy, we resolve two distinct emissive pathways: a short-lived (picosecond), right-handed CPL at 460 nm from aggregation-induced emission (AIE) species, and a long-lived (nanosecond), left-handed CPL at 520 nm from the A-TICT state. Solvent polarity dynamically governs the population balance and interconversion kinetics between the two states, inducing dual inversions in the steady-state CPL signal. This conformationally gated switching arises from the synergistic interplay of AIE and A-TICT, where structural flexibility permits excited-state evolutions inaccessible to rigid systems. Our findings provide a design principle for smart chiroptical materials with externally tunable handedness, lifetime, and temporal response, and support the applications of such materials in chiral sensing, optoelectronic devices, and dynamic information encoding.<\/jats:p>","DOI":"10.1021\/acsnano.6c10780","type":"journal-article","created":{"date-parts":[[2026,9,21]],"date-time":"2026-09-21T08:02:25Z","timestamp":1789977745000},"page":"26612-26622","source":"Crossref","is-referenced-by-count":0,"title":["Conformationally\nGated Interconversion of Photophysical\nPathways Enables Invertible Circularly Polarized Luminescence"],"prefix":"10.1021","volume":"20","author":[{"given":"Peiwen","family":"Chen","sequence":"first","affiliation":[{"name":"Tongji University , , ,","place":["Shanghai, P. R. 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China: Chem."},{"key":"2026100609081015600_cit5","doi-asserted-by":"publisher","first-page":"nwad072","DOI":"10.1093\/nsr\/nwad072","article-title":"Scale Effect\nof Circularly Polarized\nLuminescent Signal of Matter","volume":"10","author":"Sun","year":"2023","journal-title":"Natl. Sci. Rev."},{"key":"2026100609081015600_cit6","doi-asserted-by":"publisher","DOI":"10.1002\/agt2.331","article-title":"Aggregation-Induced\nEmission Polymer Systems with Circularly Polarized Luminescence","volume":"4","author":"Yan","year":"2023","journal-title":"Aggregate"},{"key":"2026100609081015600_cit7","doi-asserted-by":"publisher","first-page":"1900110","DOI":"10.1002\/adma.201900110","article-title":"Circularly Polarized\nLuminescence in Nanoassemblies: Generation, Amplification, and Application","volume":"32","author":"Sang","year":"2020","journal-title":"Adv. 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China: Chem."},{"key":"2026100609081015600_cit47","doi-asserted-by":"publisher","first-page":"40817","DOI":"10.1021\/acsami.3c10358","article-title":"Solvent-Directed Hierarchical Self-Assembly\nof Tetraphenylpyrazine-Cholesterol\nwith Amplified Circularly Polarized Luminescence","volume":"15","author":"Yao","year":"2023","journal-title":"ACS Appl. Mater. Interfaces"},{"key":"2026100609081015600_cit48","doi-asserted-by":"publisher","first-page":"94907095","DOI":"10.26599\/NR.2025.94907095","article-title":"Chirality\nInversion Via Van Der Waals Interactions to \u03c0-\u03c0 Stacking\nin Non-Equilibrium Assembly within a Narrow Temperature Range","volume":"18","author":"Chen","year":"2025","journal-title":"Nano Res."},{"key":"2026100609081015600_cit49","doi-asserted-by":"publisher","first-page":"257","DOI":"10.1016\/0009-2614(89)87592-X","article-title":"Effect of Solvent Polarity on the\nYield of Twisted Intramolecular Charge Transfer (TICT) Emission. Competition\nbetween Formation and Nonradiative Decay of the Tict State","volume":"160","author":"Nag","year":"1989","journal-title":"Chem. Phys. 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