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However, realizing anisotropic optical responses in interlayer exciton (ILE) of type-II van der Waals heterostructures has remained elusive, as most heterostructures rely on high-symmetry group-VI transition metal dichalcogenides, and attempts to introduce low-symmetry layers are hindered by interlayer momentum mismatch leading to inefficient radiative recombination. Here, we demonstrate anisotropic ILE emission in ReS2\/WS2 enabled by \u0393-point momentum matching. Polarization-resolved photoluminescence (PL) reveals three distinct ILE peaks, appearing at 1.37\u20131.42 eV for 1L-ReS2\/2L-WS2 and 1.32\u20131.37 eV for 2L-ReS2\/2L-WS2. Time-resolved, power- and temperature-dependent PL measurements, together with first-principles many-body calculations, confirm strongly anisotropic interlayer excitons from a direct \u0393-point interlayer bandgap. Furthermore, ILE intensity is independent of excitation polarization due to dominant WS2 absorption, providing a stable exciton supply for exciton transport. These findings position momentum-matched anisotropic-isotropic heterostructures as a platform for polarization-selective optoelectronics and anisotropic excitonics.<\/jats:p>","DOI":"10.1021\/acsnano.6c11574","type":"journal-article","created":{"date-parts":[[2026,9,17]],"date-time":"2026-09-17T20:02:25Z","timestamp":1789675345000},"page":"26215-26223","source":"Crossref","is-referenced-by-count":0,"title":["Anisotropic \u0393-Valley\nInterlayer Excitonic\nEmission in Anisotropic-Isotropic 2D Heterostructures"],"prefix":"10.1021","volume":"20","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-1531-1712","authenticated-orcid":true,"given":"Tae Keun","family":"Yun","sequence":"first","affiliation":[{"name":"University of California, Irvine , , , ,","place":["Irvine, California, United States, 92697"]},{"name":"Yonsei University , , ,","place":["Seoul, Korea, 03722"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Byeongchan","family":"Lee","sequence":"additional","affiliation":[{"name":"Sogang University , , ,","place":["Seoul, Korea, 04107"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Soyeong","family":"Kwon","sequence":"additional","affiliation":[{"name":"University of California, Irvine , , , ,","place":["Irvine, California, United States, 92697"]},{"name":"Kongju National University , , ,","place":["Cheonan, Korea, 31080"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0003-5448-4186","authenticated-orcid":true,"given":"Jieun","family":"Yeon","sequence":"additional","affiliation":[{"name":"Yonsei University , , ,","place":["Seoul, Korea, 03722"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0939-3731","authenticated-orcid":true,"given":"Doohee","family":"Cho","sequence":"additional","affiliation":[{"name":"Yonsei University , , ,","place":["Seoul, Korea, 03722"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4725-1299","authenticated-orcid":true,"given":"Young Woo","family":"Choi","sequence":"additional","affiliation":[{"name":"Sogang University , , ,","place":["Seoul, Korea, 04107"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8497-2330","authenticated-orcid":true,"given":"Kwanpyo","family":"Kim","sequence":"additional","affiliation":[{"name":"Yonsei University , , ,","place":["Seoul, Korea, 03722"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9719-7203","authenticated-orcid":true,"given":"SungWoo","family":"Nam","sequence":"additional","affiliation":[{"name":"University of California, Irvine , , , ,","place":["Irvine, California, United States, 92697"]},{"name":"University of California, Irvine , , , ,","place":["Irvine, California, United States, 92697"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,17]]},"reference":[{"key":"2026092909135867100_cit1","doi-asserted-by":"publisher","first-page":"372","DOI":"10.1038\/nnano.2014.35","article-title":"Black Phosphorus Field-Effect\nTransistors","volume":"9","author":"Li","year":"2014","journal-title":"Nat. Nanotechnol."},{"key":"2026092909135867100_cit2","doi-asserted-by":"publisher","first-page":"3252","DOI":"10.1038\/ncomms4252","article-title":"Monolayer Behaviour in Bulk ReS2 Due to Electronic and Vibrational Decoupling","volume":"5","author":"Tongay","year":"2014","journal-title":"Nat. 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Mater."},{"key":"2026092909135867100_cit6","doi-asserted-by":"publisher","first-page":"6198","DOI":"10.1073\/pnas.1405435111","article-title":"Strong Interlayer Coupling in van\nder Waals Heterostructures Built from Single-Layer Chalcogenides","volume":"111","author":"Fang","year":"2014","journal-title":"Proc. Natl. Acad. Sci. U. S. A."},{"key":"2026092909135867100_cit7","doi-asserted-by":"publisher","first-page":"6242","DOI":"10.1038\/ncomms7242","article-title":"Observation of Long-Lived\nInterlayer Excitons in Monolayer MoSe2-WSe2 Heterostructures","volume":"6","author":"Rivera","year":"2015","journal-title":"Nat.\nCommun."},{"key":"2026092909135867100_cit8","doi-asserted-by":"publisher","first-page":"340","DOI":"10.1038\/s41586-018-0357-y","article-title":"Room-Temperature Electrical Control of Exciton Flux in a van der\nWaals Heterostructure","volume":"560","author":"Unuchek","year":"2018","journal-title":"Nature"},{"key":"2026092909135867100_cit9","doi-asserted-by":"publisher","first-page":"870","DOI":"10.1126\/science.aaw4194","article-title":"Electrical Control\nof Interlayer Exciton Dynamics in Atomically Thin Heterostructures","volume":"366","author":"Jauregui","year":"2019","journal-title":"Science"},{"key":"2026092909135867100_cit10","doi-asserted-by":"publisher","first-page":"76","DOI":"10.1038\/s41586-019-0976-y","article-title":"Observation of Moire\u0301 Excitons in WSe2\/WS2 Heterostructure Superlattices","volume":"567","author":"Jin","year":"2019","journal-title":"Nature"},{"key":"2026092909135867100_cit11","doi-asserted-by":"publisher","first-page":"71","DOI":"10.1038\/s41586-019-0975-z","article-title":"Evidence for Moire\u0301\nExcitons in van der Waals Heterostructures","volume":"567","author":"Tran","year":"2019","journal-title":"Nature"},{"key":"2026092909135867100_cit12","doi-asserted-by":"publisher","first-page":"72","DOI":"10.1038\/s41377-021-00500-1","article-title":"Interlayer\nExciton Formation, Relaxation, and Transport in TMD van der Waals\nHeterostructures","volume":"10","author":"Jiang","year":"2021","journal-title":"Light: sci. 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Mater."},{"key":"2026092909135867100_cit23","doi-asserted-by":"publisher","first-page":"10851","DOI":"10.1039\/d2nr01973f","article-title":"Enhanced Excitonic Features in an Anisotropic ReS2\/WSe2 Heterostructure","volume":"14","author":"Usman","year":"2022","journal-title":"Nanoscale"},{"key":"2026092909135867100_cit24","doi-asserted-by":"publisher","first-page":"222101","DOI":"10.1063\/5.0170276","article-title":"Anisotropic Optical\nCharacteristics of WS2\/ReS2 Heterostructures\nwith Broken Rotational Symmetry","volume":"123","author":"Xie","year":"2023","journal-title":"Appl. Phys.\nLett."},{"key":"2026092909135867100_cit25","doi-asserted-by":"publisher","first-page":"1553","DOI":"10.1515\/nanoph-2024-0672","article-title":"Harnessing In-Plane\nOptical Anisotropy in WS2 Through ReS2 Crystal","volume":"14","author":"Kwon","year":"2025","journal-title":"Nanophotonics"},{"key":"2026092909135867100_cit26","doi-asserted-by":"publisher","first-page":"045031","DOI":"10.1088\/2053-1583\/aadf40","article-title":"Tunable Bright Interlayer Excitons\nin Few-Layer Black\nPhosphorus Based van der Waals Heterostructures","volume":"5","author":"Chen","year":"2018","journal-title":"2D Mater."},{"key":"2026092909135867100_cit27","doi-asserted-by":"publisher","first-page":"1765","DOI":"10.1021\/acs.jpclett.0c03469","article-title":"Anisotropic\nInterlayer Exciton in GeSe\/SnS van der Waals Heterostructure","volume":"12","author":"Maity","year":"2021","journal-title":"J. Phys. Chem. Lett."},{"key":"2026092909135867100_cit28","doi-asserted-by":"publisher","DOI":"10.1126\/sciadv.abq1781","article-title":"Momentum-Matching and Band-Alignment van der Waals\nHeterostructures\nfor High-Efficiency Infrared Photodetection","volume":"8","author":"Chen","year":"2022","journal-title":"Sci. Adv."},{"key":"2026092909135867100_cit29","doi-asserted-by":"publisher","first-page":"2416994","DOI":"10.1002\/adfm.202416994","article-title":"Polarization-Sensitive\nMomentum-Matching Interlayer Excitons for Infrared Photodetection","volume":"35","author":"Che","year":"2025","journal-title":"Adv. Funct. Mater."},{"key":"2026092909135867100_cit30","doi-asserted-by":"publisher","first-page":"791","DOI":"10.1021\/nn305275h","article-title":"Evolution\nof Electronic Structure\nin Atomically Thin Sheets of WS2 and WSe2","volume":"7","author":"Zhao","year":"2013","journal-title":"ACS Nano"},{"key":"2026092909135867100_cit31","doi-asserted-by":"publisher","first-page":"29","DOI":"10.1038\/s41699-018-0074-2","article-title":"Exciton Physics and Device Application of Two-Dimensional Transition\nMetal Dichalcogenide Semiconductors","volume":"2","author":"Mueller","year":"2018","journal-title":"Npj 2D\nMater. Appl."},{"key":"2026092909135867100_cit32","doi-asserted-by":"publisher","first-page":"1578","DOI":"10.1038\/s41598-018-37655-8","article-title":"Exciton Binding\nEnergy and Hydrogenic Rydberg Series in Layered ReS2","volume":"9","author":"Jadczak","year":"2019","journal-title":"Sci. Rep."},{"key":"2026092909135867100_cit33","doi-asserted-by":"publisher","first-page":"1169","DOI":"10.1002\/adfm.201504546","article-title":"Highly Sensitive Detection\nof Polarized Light Using Anisotropic 2D ReS2","volume":"26","author":"Liu","year":"2016","journal-title":"Adv. Funct. Mater."},{"key":"2026092909135867100_cit34","doi-asserted-by":"publisher","first-page":"161404(R","DOI":"10.1103\/PhysRevB.102.161404","article-title":"Additional Excitonic\nFeatures and Momentum-Dark States in ReS2","volume":"102","author":"Dhara","year":"2020","journal-title":"Phys. Rev. B"},{"key":"2026092909135867100_cit35","doi-asserted-by":"publisher","first-page":"021026","DOI":"10.1103\/PhysRevX.7.021026","article-title":"Excitonic Linewidth Approaching the\nHomogeneous Limit in MoS2-Based van der Waals Heterostructures","volume":"7","author":"Cadiz","year":"2017","journal-title":"Phys. Rev. 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B"},{"key":"2026092909135867100_cit45","doi-asserted-by":"publisher","first-page":"195438","DOI":"10.1103\/PhysRevB.99.195438","article-title":"Interlayer Charge Transfer\nin ReS2\/WS2 van der Waals Heterostructures","volume":"99","author":"Zereshki","year":"2019","journal-title":"Phys. Rev. B"},{"key":"2026092909135867100_cit46","doi-asserted-by":"publisher","first-page":"5187","DOI":"10.1021\/acs.nanolett.7b00627","article-title":"Direct Observation of the Band Gap\nTransition in Atomically Thin ReS2","volume":"17","author":"Gehlmann","year":"2017","journal-title":"Nano Lett."},{"key":"2026092909135867100_cit47","doi-asserted-by":"publisher","first-page":"035125","DOI":"10.1103\/PhysRevB.94.035125","article-title":"Band Alignment\nof Two-Dimensional Semiconductors for Designing Heterostructures with\nMomentum Space Matching","volume":"94","author":"O\u0308zc\u0327elik","year":"2016","journal-title":"Phys. Rev. B"},{"key":"2026092909135867100_cit48","doi-asserted-by":"publisher","first-page":"5627","DOI":"10.1021\/nl403270k","article-title":"Origin of Indirect Optical Transitions\nin Few-Layer MoS2, WS2, and WSe2","volume":"13","author":"Zhao","year":"2013","journal-title":"Nano Lett."},{"key":"2026092909135867100_cit49","doi-asserted-by":"publisher","first-page":"54808","DOI":"10.1021\/acsami.3c12429","article-title":"Observation\nof Strong Anisotropic Interlayer Excitons","volume":"15","author":"Luo","year":"2023","journal-title":"ACS\nAppl. Mater. Interfaces"},{"key":"2026092909135867100_cit50","doi-asserted-by":"publisher","first-page":"8643","DOI":"10.1021\/acs.nanolett.3c02488","article-title":"Ultrafast Electronic\nDynamics in Anisotropic Indirect Interlayer Excitonic States of Monolayer\nWSe2\/ReS2 Heterojunctions","volume":"23","author":"Qin","year":"2023","journal-title":"Nano Lett."},{"key":"2026092909135867100_cit51","doi-asserted-by":"publisher","first-page":"1068","DOI":"10.1038\/s41563-020-0730-8","article-title":"Excitons in Strain-Induced\nOne-Dimensional Moire\u0301\nPotentials at Transition Metal Dichalcogenide Heterojunctions","volume":"19","author":"Bai","year":"2020","journal-title":"Nat. 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