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Both ILs promoted the complete dissolution of cellulose, with the process in [Emim]\u00adOAc occurring faster and with less fiber swelling. The obtained filaments exhibited a homogeneous appearance and a dense morphology, and it was noted that the optical brightener present in the cotton residue was maintained in the filament composition. The dissolution and regeneration processes promoted the depolymerization of cellulose, with significant differences between the ILs and the coagulant. The highest depolymerization was observed for the filaments resulting from the dissolution in [Emim]\u00adCl. X-ray diffraction analysis indicated a change in the crystalline structure of cellulose I of the residue to an amorphous structure in the filaments, except for the filament from dissolution in [Emim]\u00adOAc and coagulation in ethanol, which presented a type II cellulose structure. Thermal stability was reduced for all filaments, with the lowest degradation temperature observed for the filament from dissolution in [Emim]Cl and coagulation in ethanol. This filament also obtained inferior mechanical properties as a result of low DP and crystallinity. The elastic modulus of the other filaments (10\u201313 GPa) was similar to that of regenerated fibers such as viscose and modal. Among the IL-coagulant systems evaluated, [Emim]\u00adOAc-ethanol resulted in the most promising mechanical, thermal, and morphological properties.<\/jats:p>","DOI":"10.1021\/acsomega.5c01867","type":"journal-article","created":{"date-parts":[[2025,5,7]],"date-time":"2025-05-07T04:59:40Z","timestamp":1746593980000},"page":"19983-19991","source":"Crossref","is-referenced-by-count":8,"title":["Regenerated Cellulose\nFilaments from the Recycling\nof Textile Cotton Waste Using Ionic Liquids"],"prefix":"10.1021","volume":"10","author":[{"given":"Beatriz","family":"Barbosa de Brito","sequence":"first","affiliation":[{"name":"Federal University of Santa Catarina, UFSC , , Joa\u0303o Pessoa 2750 , , ,","place":["Blumenau, Santa Catarina, Brazil, 89036-256"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Beatriz","family":"Kru\u0308ger","sequence":"additional","affiliation":[{"name":"Federal University of Santa Catarina, UFSC , , Joa\u0303o Pessoa 2750 , , ,","place":["Blumenau, Santa Catarina, Brazil, 89036-256"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lucas","family":"Souza da Silva","sequence":"additional","affiliation":[{"name":"Federal University of Santa Catarina, UFSC , , Joa\u0303o Pessoa 2750 , , ,","place":["Blumenau, Santa Catarina, Brazil, 89036-256"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Cintia","family":"Marangoni","sequence":"additional","affiliation":[{"name":"Federal University of Santa Catarina, UFSC , , Eng. Agrono\u0302mico Andrei Cristian Ferreira s\/n , , ,","place":["Floriano\u0301polis, Santa Catarina, Brazil, 88040-900"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7133-1590","authenticated-orcid":true,"given":"Andrea","family":"Cristiane Krause Bierhalz","sequence":"additional","affiliation":[{"name":"Federal University of Santa Catarina, UFSC , , Joa\u0303o Pessoa 2750 , , ,","place":["Blumenau, Santa Catarina, Brazil, 89036-256"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2025,5,7]]},"reference":[{"issue":"2","key":"2026081811223471400_cit1","doi-asserted-by":"publisher","first-page":"335","DOI":"10.1039\/D2SU00084A","article-title":"Upcycling\nof Textile Waste into High Added Value Cellulose Porous Materials,\nAerogels and Cryogels","volume":"1","author":"Ne\u0301grier","year":"2023","journal-title":"RSC Sustain"},{"issue":"1","key":"2026081811223471400_cit2","doi-asserted-by":"publisher","DOI":"10.1016\/j.heliyon.2023.e23834","article-title":"Impact\nof Vitamin E in Improving Comfort, Moisture Management and Mechanical\nProperties of Flame-Retardant Treated Cotton Fabric","volume":"10","author":"Moula","year":"2024","journal-title":"Heliyon"},{"key":"2026081811223471400_cit3","doi-asserted-by":"publisher","first-page":"163659","DOI":"10.1016\/j.scitotenv.2023.163659","article-title":"A Systematic Review of the Life Cycle\nEnvironmental Performance of Cotton Textile Products","volume":"883","author":"Chen","year":"2023","journal-title":"Sci. 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