{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,8,18]],"date-time":"2026-08-18T18:24:15Z","timestamp":1787077455418,"version":"build-2736575974"},"reference-count":57,"publisher":"American Chemical Society (ACS)","issue":"25","license":[{"start":{"date-parts":[[2025,6,19]],"date-time":"2025-06-19T00:00:00Z","timestamp":1750291200000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by-nc-nd\/4.0\/"}],"funder":[{"DOI":"10.13039\/na","name":"SECIHTI","doi-asserted-by":"publisher","award":["588460"],"award-info":[{"award-number":["588460"]}],"id":[{"id":"10.13039\/na","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2025,7,1]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>Exposure to pesticides is associated with harmful effects on the environment and public health. There is an urgent need to develop alternative detection methods to ensure that water supply sources remain free from pesticides. In this work, an iron terephthalate metal\u2013organic framework from the family MIL-101 was studied as an alternative adsorbent for the fabrication of hybrid solid-phase extraction (SPE) cartridges for the determination of glyphosate and aminomethyl-phosphonic acid (AMPA) in tap and river water samples by chromatographic analysis. Hybrid cartridges were fabricated based on synthesized MIL-101\u00ad(Fe) by a microwave-assisted method and packed with silica C18 inside empty commercial cartridges. Then, the general conditions for the SPE of selected pesticides were studied in detail. The proposed SPE methodology enabled the achievement of improved analytical results compared to conventional adsorbents, including limits of detection of 1.2 and 3.9 ng\/mL, along with enrichment factors of 27.7 and 56 for GLY and AMPA, respectively. Extraction recoveries ranged from 76% to 108%, with satisfactory relative standard deviation values below 3.5% (intraday precision, n = 5) and 9.4% (interday precision, n = 5). Linear ranges were observed from 10 to 1000 ng\/mL, with determination coefficients exceeding 0.997. The obtained results suggest the successful employment of MIL-101\u00ad(Fe) in alternative and practical methodologies for the pretreatment of water samples, facilitating the determination of pesticides and diminishing the harmful impacts of derivatization steps.<\/jats:p>","DOI":"10.1021\/acsomega.5c03322","type":"journal-article","created":{"date-parts":[[2025,6,19]],"date-time":"2025-06-19T06:24:31Z","timestamp":1750314271000},"page":"27483-27490","source":"Crossref","is-referenced-by-count":2,"title":["Hybrid Cartridges\nBased on Metal\u2013Organic Frameworks:\nA Cost-Reducing and Sensitive Green Alternative for the Detection\nof Glyphosate and Its Metabolite AMPA"],"prefix":"10.1021","volume":"10","author":[{"given":"Gabriela","family":"Pen\u0303a-Velasco","sequence":"first","affiliation":[{"name":"University of Guadalajara , , Marcelino Garcia Barragan Street, Number 1451 , , ,","place":["Guadalajara, Jalisco, Mexico, 44430"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ismael Alejandro","family":"Aguayo-Villarreal","sequence":"additional","affiliation":[{"name":"University of Colima , , Km 9 Colima-Coquimatla\u0301n Highway , , ,","place":["Coquimatla\u0301n, Colima, Mexico, 28400"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Rosa Mari\u0301a","family":"Jime\u0301nez-Amezcua","sequence":"additional","affiliation":[{"name":"University of Guadalajara , , Marcelino Garcia Barragan Street, Number 1451 , , ,","place":["Guadalajara, Jalisco, Mexico, 44430"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Francisco Jose\u0301","family":"Aranda-Garci\u0301a","sequence":"additional","affiliation":[{"name":"University of Guadalajara , , Av. Independencia Nacional Number 151 , , ,","place":["Autla\u0301n, Jalisco, Mexico, 48900"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7149-8243","authenticated-orcid":true,"given":"Alejandro Aaro\u0301n","family":"Peregrina-Lucano","sequence":"additional","affiliation":[{"name":"University of Guadalajara , , Marcelino Garcia Barragan Street, Number 1451 , , ,","place":["Guadalajara, Jalisco, Mexico, 44430"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2025,6,19]]},"reference":[{"key":"2026081811275915700_cit1","doi-asserted-by":"publisher","first-page":"1121","DOI":"10.1007\/s10337-019-03748-3","article-title":"Solid-Phase Extraction\nof Glyphosate in the Analyses of Environmental, Plant, and Food Samples","volume":"82","author":"Rigobello-Masini","year":"2019","journal-title":"Chromatographia"},{"key":"2026081811275915700_cit2","doi-asserted-by":"publisher","first-page":"592","DOI":"10.1080\/19440049.2019.1583380","article-title":"Detection of glyphosate\nand its metabolites in food of animal origin based on ion-chromatography-high\nresolution mass spectrometry (IC-HRMS)","volume":"36","author":"Chiesa","year":"2019","journal-title":"Food\nAddit. Contam., Part A: Chem., Anal., Control, Exposure Risk Assess."},{"key":"2026081811275915700_cit3","doi-asserted-by":"publisher","first-page":"29","DOI":"10.20937\/RICA.2018.34.esp01.03","article-title":"Estado actual de la investigacio\u0301n\nsobre plaguicidas en Me\u0301xico","volume":"34","author":"Garci\u0301a\nHerna\u0301ndez","year":"2018","journal-title":"Rev. Int.\nContam. Ambiental"},{"key":"2026081811275915700_cit4","doi-asserted-by":"publisher","first-page":"135","DOI":"10.1016\/j.jes.2018.11.019","article-title":"Temporal trends in\norganophosphorus pesticides use and concentrations in river water\nin Japan, and risk assessment","volume":"79","author":"Derbalah","year":"2019","journal-title":"J. Environ. 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