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In this study, a virtual electronic tongue combining electrochemical impedance spectroscopy (EIS) and artificial neural networks (ANNs) was applied to identify and quantify common gasoline adulterants, namely, n-hexane, toluene, and mineral turpentine, in single- and multiadulterant systems. Measurements were performed using a glassy carbon electrode with platinum counter and pseudoreference electrodes. Single-adulterant systems exhibited increasing Nyquist semicircle diameters in the order n-hexane &amp;lt; mineral turpentine &amp;lt; toluene, while binary and ternary mixtures showed nonmonotonic impedance behavior, reflecting concentration-dependent intermolecular interactions. ANN models trained with the imaginary impedance component (Z\u2033) demonstrated improved performance when restricted to the semicircle region of the Nyquist plots. This approach resulted in no misclassifications in the test set for adulterant type and enhanced regression performance for individual adulterants, even in mixed systems (test-set R2 = 0.846 for n-hexane, 0.965 for toluene, and 0.742 for mineral turpentine). These results show that focusing on the semicircle domain concentrates the most informative impedance features and enables reliable identification and quantification of gasoline adulteration while also revealing the inherent complexity of multiadulterant fuel systems.<\/jats:p>","DOI":"10.1021\/acsomega.5c08979","type":"journal-article","created":{"date-parts":[[2026,2,27]],"date-time":"2026-02-27T06:39:41Z","timestamp":1772174381000},"page":"14381-14391","source":"Crossref","is-referenced-by-count":0,"title":["Virtual Electronic\nTongue Combining Electrochemical\nImpedance Spectroscopy and the Artificial Neural Network for Accurate\nIdentification of Noncompliant Gasoline"],"prefix":"10.1021","volume":"11","author":[{"given":"Bianca\nde Paula","family":"Cola","sequence":"first","affiliation":[{"name":"Universidade Federal do Rio de Janeiro , , , ,","place":["Rio de Janeiro, RJ, Brazil, 21941-909"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Andre\u0301 Guimara\u0303es de","family":"Oliveira","sequence":"additional","affiliation":[{"name":"UFRJ, Universidade Federal do Rio de Janeiro, Centro de Tecnologia , , Bloco E , , ,","place":["Rio de Janeiro, RJ, Brazil, 21941-909"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ana Maria","family":"Rocco","sequence":"additional","affiliation":[{"name":"UFRJ, Universidade Federal do Rio de Janeiro, Centro de Tecnologia , , Bloco E , , ,","place":["Rio de Janeiro, RJ, Brazil, 21941-909"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0581-2038","authenticated-orcid":true,"given":"Maiara Oliveira","family":"Salles","sequence":"additional","affiliation":[{"name":"Universidade Federal do Rio de Janeiro , , , ,","place":["Rio de Janeiro, RJ, Brazil, 21941-909"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,2,27]]},"reference":[{"key":"2026081508072668600_cit1","doi-asserted-by":"publisher","first-page":"135405","DOI":"10.1016\/j.fuel.2025.135405","article-title":"Identification and Classification\nof Adulteration in Some Fossil Fuel Products Using an Electronic Nose","volume":"396","author":"Kakaei","year":"2025","journal-title":"Fuel"},{"key":"2026081508072668600_cit2","doi-asserted-by":"publisher","first-page":"38","DOI":"10.1016\/j.fuel.2017.02.066","article-title":"QCM Virtual\nMultisensor Array for Fuel Discrimination and Detection of Gasoline\nAdulteration","volume":"199","author":"Speller","year":"2017","journal-title":"Fuel"},{"issue":"10\u201311","key":"2026081508072668600_cit3","doi-asserted-by":"publisher","first-page":"2168","DOI":"10.1016\/j.fuel.2007.11.003","article-title":"Influence\nof Solvent Addition on the Physicochemical Properties of Brazilian\nGasoline","volume":"87","author":"Takeshita","year":"2008","journal-title":"Fuel"},{"key":"2026081508072668600_cit4","doi-asserted-by":"publisher","first-page":"1","DOI":"10.1016\/j.trac.2017.04.011","article-title":"Monitoring Petroleum\nFuel Adulteration: A Review of\nAnalytical Methods","volume":"92","author":"Vempatapu","year":"2017","journal-title":"TrAC Trends in Analytical\nChemistry"},{"key":"2026081508072668600_cit5","doi-asserted-by":"publisher","first-page":"122754","DOI":"10.1016\/j.fuel.2021.122754","article-title":"Impact of Diesel and\nDetergent Contamination on Gasoline Low-Speed Pre-Ignition and Their\nCharacterization Using Unwashed Gums","volume":"318","author":"Colliou","year":"2022","journal-title":"Fuel"},{"issue":"4","key":"2026081508072668600_cit6","doi-asserted-by":"publisher","first-page":"467","DOI":"10.1016\/j.fuel.2004.09.013","article-title":"Adulteration\nDetection of Brazilian\nGasoline Samples by Statistical Analysis","volume":"84","author":"Wiedemann","year":"2005","journal-title":"Fuel"},{"key":"2026081508072668600_cit7","unstructured":"Age\u0302ncia\nNacional do Petro\u0301leo, G. 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