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The immobilized catalyst exhibited a H2 production rate of approximately 14 \u03bcmol cm\u20132 h\u20131 at 40 \u00b0C, achieving performance comparable to slurry-based systems while eliminating the need for postreaction separation of the photocatalyst. Hydrogen evolution yields were primarily governed by photon energy, catalyst loading, and substrate concentration, whereas the cumulative hydrogen yield remained similar within the investigated temperature range (40\u201380 \u00b0C), despite differences in the initial reaction profile and catalyst stability observed at 80 \u00b0C. The catalyst demonstrated a stable performance under the tested experimental conditions, maintaining constant activity over 10 consecutive reuse cycles with no detectable loss of immobilized mass. Liquid-phase analysis revealed that the detected products were consistent with oxidative cleavage reactions during cellobiose photoreforming, leading to formic acid and formaldehyde as the main detected products. Overall, the results indicate that the immobilized TiO2@Pt(0.5) photocatalyst demonstrates potential as an effective proof-of-concept material for biomass photoreforming in an immobilized configuration and warrants further optimization and mechanistic investigation.<\/jats:p>","DOI":"10.1021\/acsomega.6c01812","type":"journal-article","created":{"date-parts":[[2026,8,9]],"date-time":"2026-08-09T14:01:58Z","timestamp":1786284118000},"page":"49214-49224","source":"Crossref","is-referenced-by-count":0,"title":["Photocatalytic\nHydrogen Production from Cellobiose\nUsing TiO2@Pt(0.5) Immobilized Photocatalyst"],"prefix":"10.1021","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-9858-7836","authenticated-orcid":true,"given":"Bruno C. B.","family":"Salgado","sequence":"first","affiliation":[{"name":"Federal Institute of Ceara ., Av. Parque Central, 1315 , , ,","place":["Maracanau, Ceara, Brazil, 61939-140"]},{"name":"Queen\u2019s University Belfast , , Stranmillis Road , ,","place":["Belfast, United Kingdom, BT9 5AG"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5922-9761","authenticated-orcid":true,"given":"Mayara M. R.","family":"Oliveira","sequence":"additional","affiliation":[{"name":"Federal Institute of Ceara ., Av. 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