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Among the various cathode candidates, Prussian blue analogs (PBAs) stand out due to their tunable chemistry, open-framework structure, and low production costs. However, conventional PBAs typically exhibit limited rate performance, leading to poor capacity retention and reduced cycle life. In this work, we present a straightforward coprecipitation synthesis of a novel zinc nitroprusside, Zn[Fe(CN)5NO], in which zinc incorporation enhances the structural stability of the large-channel framework, directly addressing the intrinsic limitations of traditional PBAs. The material exhibited remarkable structural stability under high-voltage operation (4.5 V), delivering excellent rate performance with 79% capacity retention after 500 cycles at 91 mA g\u20131 (1C), alongside a maximum discharge capacity of 69.4 mA h g\u20131 at 9.1 mA g\u20131 (0.1C). This study advances the development of stable, cost-effective cathode materials for NIBs. It highlights the potential of zinc-stabilized frameworks in enabling both high electrochemical performance and long-term cycling stability, representing a step toward wider adoption of NIB technology.<\/jats:p>","DOI":"10.1021\/acsomega.6c02046","type":"journal-article","created":{"date-parts":[[2026,9,10]],"date-time":"2026-09-10T01:02:09Z","timestamp":1789002129000},"page":"55111-55125","source":"Crossref","is-referenced-by-count":0,"title":["Ultra-Stable Zinc\nNitroprusside Cathode Operating\nat High Potentials for Inexpensive, Simpler-to-Scale Sodium-Ion Batteries"],"prefix":"10.1021","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-5471-4760","authenticated-orcid":true,"given":"Joa\u0303o F. M.","family":"Alves","sequence":"first","affiliation":[{"name":"University of Porto , , Rua Dr. Roberto Frias , ,","place":["Porto, Portugal, 4200-465"]},{"name":"University of Coimbra , , Po\u0301lo II, Pinhal de Marrocos , ,","place":["Coimbra, Portugal, 3004-504"]},{"name":"University of Coimbra , , Po\u0301lo II, Pinhal de Marrocos , ,","place":["Coimbra, Portugal, 3004-504"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hugo","family":"Cruz","sequence":"additional","affiliation":[{"name":"University of Porto , , Rua Dr. Roberto Frias , ,","place":["Porto, Portugal, 4200-465"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Miguel","family":"Duarte","sequence":"additional","affiliation":[{"name":"University of Porto , , Rua Dr. Roberto Frias , ,","place":["Porto, Portugal, 4200-465"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8091-1212","authenticated-orcid":true,"given":"Yonny","family":"Romaguera-Barcelay","sequence":"additional","affiliation":[{"name":"University of Coimbra , , Po\u0301lo II, Pinhal de Marrocos , ,","place":["Coimbra, Portugal, 3004-504"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6493-0237","authenticated-orcid":true,"given":"Walter R.","family":"Brito","sequence":"additional","affiliation":[{"name":"University of Coimbra , , Po\u0301lo II, Pinhal de Marrocos , ,","place":["Coimbra, Portugal, 3004-504"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Teo\u0301filo","family":"Rojo","sequence":"additional","affiliation":[{"name":"University of the Basque Country UPV\/EHU , , ,","place":["Bilbao, Spain, 48013"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jorge F. J.","family":"Coelho","sequence":"additional","affiliation":[{"name":"University of Coimbra , , Po\u0301lo II, Pinhal de Marrocos , ,","place":["Coimbra, Portugal, 3004-504"]},{"name":"IPN, Instituto Pedro Nunes , , Rua Pedro Nunes , ,","place":["Coimbra, Portugal, 3030-199"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2472-3265","authenticated-orcid":true,"given":"Ade\u0301lio M.","family":"Mendes","sequence":"additional","affiliation":[{"name":"University of Porto , , Rua Dr. Roberto Frias , ,","place":["Porto, Portugal, 4200-465"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-9936-7336","authenticated-orcid":true,"given":"M. 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