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To address this, we report a conceptual and methodological advance by developing a brand-new \u201cneedle-confined region free-surface\u201d triaxial electrospinning process. In a unique waste-to-resource concept, discarded polyethylene terephthalate (PET) beverage bottles were innovatively converted into the multifluid spinneret. This scalable device was utilized to batch-fabricate surface-porous core\u2013sheath nanofibers using waste polystyrene (PS) foam as the primary matrix. These nanofibers comprised a porous PS\/TiO2 sheath to maximize catalytic exposure, while the polyacrylonitrile (PAN) core endowed the nanofibers with robust mechanical properties. As a proof of concept for this manufacturing approach, the resultant membranes were applied to antibiotic wastewater treatment, exhibiting excellent hydrophilicity, enhanced mechanical properties, and a high specific surface area with pronounced surface porosity. In a simulated tetracycline wastewater solution (pH 8), their photocatalytic degradation efficiency reached 70.05% within 2 h and was maintained at 66.74% after four reuse cycles. Beyond simply engineering a specific functional membrane, this integration of needle-based and free-surface electrospinning establishes a straightforward platform for the one-step scalable batch production of various multichamber nanostructures, providing robust support for advanced nanomaterials fabrication.<\/jats:p>","DOI":"10.1021\/acsomega.6c03877","type":"journal-article","created":{"date-parts":[[2026,7,16]],"date-time":"2026-07-16T20:54:03Z","timestamp":1784235243000},"page":"44015-44028","source":"Crossref","is-referenced-by-count":15,"title":["Scalable and Systematical\nConversions of Domestic\nWastes to Core\u2013Sheath Nanofibers for Photocatalytic Degradation\nof Antibiotics"],"prefix":"10.1021","volume":"11","author":[{"given":"Ran","family":"Dong","sequence":"first","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yingao","family":"Ru","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xinyi","family":"Zhang","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jiaqi","family":"Zhu","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Haifeng","family":"Wen","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Daihua","family":"He","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7825-4498","authenticated-orcid":true,"given":"Deng-Guang","family":"Yu","sequence":"additional","affiliation":[{"name":"University of Shanghai for Science and Technology , , ,","place":["Shanghai, China, 200093"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,7,16]]},"reference":[{"key":"2026072810120979600_cit1","doi-asserted-by":"publisher","first-page":"22441","DOI":"10.1021\/acsomega.6c00310","article-title":"Engineered Nanomaterial-Based\nPhotocatalysts for Efficient and Sustainable Degradation of Antibiotics\nin Water: A Review","volume":"11","author":"Rawat","year":"2026","journal-title":"ACS Omega"},{"issue":"2","key":"2026072810120979600_cit2","doi-asserted-by":"publisher","first-page":"345","DOI":"10.1007\/s10311-019-00945-2","article-title":"Remediation\nof Wastewater Contaminated by Antibiotics. 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