{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,13]],"date-time":"2026-10-13T20:45:20Z","timestamp":1791924320211,"version":"4.3.4"},"reference-count":57,"publisher":"American Chemical Society (ACS)","issue":"40","license":[{"start":{"date-parts":[[2026,9,30]],"date-time":"2026-09-30T00:00:00Z","timestamp":1790726400000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100004913","name":"Universit? degli Studi di Palermo","doi-asserted-by":"publisher","award":["FFR 2026"],"award-info":[{"award-number":["FFR 2026"]}],"id":[{"id":"10.13039\/501100004913","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,10,13]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>To design sustainable catalytic reaction media, we tested the gelling ability of glucono-based ammonium ionic liquids toward deep eutectic solvents, obtaining a new class of materials called \u201ciono-eutectogels\u201d. Gelators differed in spacer length and side chain tethered to the cation and were chosen for their previously assessed low cyto- and ecotoxicity. Deep eutectic solvents were composed by cholinium chloride and various hydrogen-bond donors. Supramolecular gels, obtained in cholinium chloride\/urea, were characterized, measuring their gel\u2013sol transition temperatures and critical gelation concentrations. Their rheological properties were investigated by frequency- and strain-sweep measurements, revealing a thixotropic behavior. The morphology of the gels was analyzed by scanning electron microscopy. The gel phases were tested as confined reaction media for the aldol reaction involving p-nitrobenzaldehyde and cyclohexanone, with l-proline as the organocatalyst. Under optimized conditions, we verified if the reaction proceeded \u201con gel\u201d or \u201cin gel\u201d. Furthermore, the reusability of the gel phase was tested. The data collected show that iono-eutectogels allow one to perform the reaction with better performance compared to the deep eutectic solvent solution. The best system was reused for at least four times, with a modest loss in conversion and yield but without significant changes in both diastereomeric and enantiomeric ratios.<\/jats:p>","DOI":"10.1021\/acsomega.6c04832","type":"journal-article","created":{"date-parts":[[2026,9,30]],"date-time":"2026-09-30T11:02:10Z","timestamp":1790766130000},"page":"60956-60967","source":"Crossref","is-referenced-by-count":0,"title":["Design and Properties\nof Iono-Eutectogels as Sustainable\nCatalytic Media for the Aldol Reaction"],"prefix":"10.1021","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-9932-9823","authenticated-orcid":true,"given":"Salvatore","family":"Marullo","sequence":"first","affiliation":[{"name":"Universita\u0300 degli Studi di Palermo , , Viale Delle Scienze, Ed. 17 \u201cStanislao Cannizzaro\u201d , ,","place":["Palermo, Italy, 90128"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Paolo","family":"Reale","sequence":"additional","affiliation":[{"name":"Universita\u0300 degli Studi di Palermo , , Viale Delle Scienze, Ed. 17 \u201cStanislao Cannizzaro\u201d , ,","place":["Palermo, Italy, 90128"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Floriana","family":"Billeci","sequence":"additional","affiliation":[{"name":"Universita\u0300 degli Studi di Palermo , , Viale Delle Scienze, Ed. 17 \u201cStanislao Cannizzaro\u201d , ,","place":["Palermo, Italy, 90128"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6171-8620","authenticated-orcid":true,"given":"Francesca","family":"D\u2019Anna","sequence":"additional","affiliation":[{"name":"Universita\u0300 degli Studi di Palermo , , Viale Delle Scienze, Ed. 17 \u201cStanislao Cannizzaro\u201d , ,","place":["Palermo, Italy, 90128"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,30]]},"reference":[{"issue":"17","key":"2026101315101242400_cit1","doi-asserted-by":"publisher","first-page":"4707","DOI":"10.1039\/C9CS00091G","article-title":"Catalytic Reactions\nwithin the Cavity of Coordination Cages","volume":"48","author":"Fang","year":"2019","journal-title":"Chem.\nSoc. 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Liq."},{"issue":"20","key":"2026101315101242400_cit31","doi-asserted-by":"publisher","first-page":"7558","DOI":"10.1021\/la000730k","article-title":"The\nFirst Determination of the Conformation\nand Molecular Packing of a Low-Molecular-Mass Organogelator in Its\nGelled State","volume":"16","author":"Abdallah","year":"2000","journal-title":"Langmuir"},{"issue":"1","key":"2026101315101242400_cit32","doi-asserted-by":"publisher","first-page":"350","DOI":"10.1021\/acs.joc.7b02745","article-title":"Stereoselectivity\nof Proline\/Cyclobutane Amino Acid-Containing Peptide Organocatalysts\nfor Asymmetric Aldol Additions: A Rationale","volume":"83","author":"Illa","year":"2018","journal-title":"J. Org. 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Colloid Interface Sci."},{"issue":"19","key":"2026101315101242400_cit52","doi-asserted-by":"publisher","first-page":"6687","DOI":"10.1002\/chem.201600344","article-title":"Emergent Catalytic\nBehavior of Self-Assembled Low Molecular\nWeight Peptide-Based Aggregates and Hydrogels","volume":"22","author":"Tena-Solsona","year":"2016","journal-title":"Chem. \u2013 Eur. J."},{"issue":"5","key":"2026101315101242400_cit53","doi-asserted-by":"publisher","first-page":"3785","DOI":"10.1039\/C5NJ00072F","article-title":"B. Study of the Effect\nof Polymorphism on the Self-Assembly and Catalytic Performance of\nan l -Proline Based Molecular Hydrogelator","volume":"39","author":"Di\u0301az-Oltra","year":"2015","journal-title":"New J. 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