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Herein, ZIF-8 was deliberately grown in situ on PAN\/PVP nanofiber using an electrospinning technique to attain a hierarchically porous architecture. The integration of ZIF-8 templates and the thermal decomposition of PVP created a network of interconnected micropores and mesopores, yielding a Brunauer\u2013Emmett\u2013Teller (BET) specific surface area of 373.18 m2 g\u20131 and a maximum pore volume of 0.28 cm2 g\u20131. X-ray photoelectron spectroscopy (XPS) confirmed successful nitrogen doping, which significantly enhanced pseudocapacitive behavior, surface wettability, and charge-transfer kinetics in an acidic medium. The dominant surface-controlled capacitive storage mechanism (65\u201394%) makes the C-ZNF electrode exhibit a high specific capacitance of 278 F g\u20131 at 1 A g\u20131 in 1 M H2SO4. This unique architecture facilitates effective ion transport pathways and improves the charge storage mechanism by reducing internal resistance at the electrode\u2013electrolyte interface. Furthermore, the symmetric coin cell-assembled device exhibits higher power density and energy density of 1000 W kg\u20131 and 34 Wh kg\u20131, respectively. The device exhibited a maximum specific capacitance of 340 F g\u20131 at a current density of 0.3 A g\u20131 (C-ZNF \/\/ C-ZNF). The device retained 84% of its initial capacitance after 5000 charge\u2013discharge cycles. These findings demonstrate the potential of ZIF-8-derived carbon nanofiber as a promising electrode material for high-performance supercapacitors.<\/jats:p>","DOI":"10.1021\/acsomega.6c05089","type":"journal-article","created":{"date-parts":[[2026,9,12]],"date-time":"2026-09-12T01:01:32Z","timestamp":1789174892000},"page":"55727-55738","source":"Crossref","is-referenced-by-count":1,"title":["Non-Coalesced ZIF-8\nMOF-Derived Hierarchical\nPorous Carbon Nanofibers for Energy Storage Applications"],"prefix":"10.1021","volume":"11","author":[{"given":"Sivasri","family":"Babu","sequence":"first","affiliation":[{"name":"Vellore Institute of Technology , , ,","place":["Vellore, India, 632 014"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8714-1716","authenticated-orcid":true,"given":"Andrews Nirmala","family":"Grace","sequence":"additional","affiliation":[{"name":"Vellore Institute of Technology , , ,","place":["Vellore, India, 632 014"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,11]]},"reference":[{"issue":"March","key":"2026092210573811800_cit1","doi-asserted-by":"publisher","first-page":"106950","DOI":"10.1016\/j.resconrec.2023.106950","article-title":"Greenhouse\nGas Emissions, Land Use and Employment in a Future Global Bioplastics\nEconomy","volume":"193","author":"Jin","year":"2023","journal-title":"Resour., Conserv. 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