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In this work, Cu oxide nanoparticles were confined in three distinct supports: MCF (mesocellular foam) silica, layers of carbon nitride on the surface of mesoporous silica (MCF-CN), or layers of P-doped carbon nitride (MCF-CN-P). The carbon nitride coating was produced using cyanamide, and P-doped carbon nitride was created from a mixture of cyanamide and sodium hypophosphite. The different supports were used to investigate their effects on the distribution, size, and stability of Cu-based particles in the selective oxidation of alcohols, employing peroxymonosulfate (PMS) as the oxidizing agent. Primary and secondary alcohols such as cyclohexanol, benzyl alcohol, and 4-hydroxy-3,5-dimethoxybenzyl alcohol were used as substrates. The synthesized layers of P-doped carbon nitride enhance the conversion of alcohols to their respective ketones or aldehydes, achieving conversions above 80% and selectivity above 90%. Moreover, the stability of copper oxide increases compared with particles deposited on pristine silica.<\/jats:p>","DOI":"10.1021\/acsomega.6c05865","type":"journal-article","created":{"date-parts":[[2026,8,4]],"date-time":"2026-08-04T14:33:59Z","timestamp":1785854039000},"page":"48563-48573","source":"Crossref","is-referenced-by-count":0,"title":["Copper Nanoparticle\nConfinement in P-Doped\nCarbon Nitride Templates Enables Efficient Peroxymonosulfate Activation\nfor Alcohol Oxidation"],"prefix":"10.1021","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-7611-9751","authenticated-orcid":true,"given":"Rafael L.","family":"Oliveira","sequence":"first","affiliation":[{"name":"Institute of Low Temperature and Structure Research of the Polish Academy of Sciences , ,","place":["Wroclaw, Poland, 50422"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3152-8070","authenticated-orcid":true,"given":"Emilia","family":"Witkowska-Nery","sequence":"additional","affiliation":[{"name":"Institute of Physical Chemistry of the Polish Academy of Sciences , ,","place":["Warsaw, Poland, 01-224"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6852-7616","authenticated-orcid":true,"given":"Sebastian","family":"Praetz","sequence":"additional","affiliation":[{"name":"Technical University Berlin , , ,","place":["Berlin, Germany, 10623"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Christopher","family":"Schlesiger","sequence":"additional","affiliation":[{"name":"Technical University Berlin , , ,","place":["Berlin, Germany, 10623"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,3]]},"reference":[{"issue":"14","key":"2026081811130623500_cit1","doi-asserted-by":"publisher","first-page":"4297","DOI":"10.1002\/slct.202000829","article-title":"Hydroxyapatite-Supported Manganese Oxides as Efficient Non-Noble-Metal\nCatalysts for Selective Aerobic Oxidation of Alcohols","volume":"5","author":"Chen","year":"2020","journal-title":"ChemistrySelect"},{"issue":"3","key":"2026081811130623500_cit2","doi-asserted-by":"publisher","first-page":"550","DOI":"10.1039\/C8RE00212F","article-title":"Continuous\nFlow Aerobic Alcohol Oxidation Using a Heterogeneous Ru 0 Catalyst","volume":"4","author":"Sofack Kreutzer","year":"2019","journal-title":"React. 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