{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,13]],"date-time":"2026-10-13T20:44:57Z","timestamp":1791924297803,"version":"4.3.4"},"reference-count":107,"publisher":"American Chemical Society (ACS)","issue":"40","license":[{"start":{"date-parts":[[2026,10,2]],"date-time":"2026-10-02T00:00:00Z","timestamp":1790899200000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by-nc-nd\/4.0\/"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,10,13]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>A novel isoxazolone derivative, (E)-4-(4-(diethylamino)benzylidene)-3-methylisoxazol-5(4H)-one (DEAI), was synthesized via a one-pot, environmentally friendly protocol and characterized by spectroscopic techniques. Its corrosion inhibition performance toward carbon steel in 1 M HCl was investigated using electrochemical methods, including potentiodynamic polarization and electrochemical impedance spectroscopy, combined with surface analyses (AFM, XPS, UPS) and theoretical calculations. Electrochemical results indicate that DEAI acts as a mixed-type inhibitor with predominant cathodic behavior, achieving maximum inhibition efficiencies of 87.5% (303 K), 88.1% (308 K), 92.7% (313 K), 90.2% (318 K), and 86.7% (323 K) at 7.5 \u00d7 10\u20135 M. Impedance measurements reveal that the corrosion process is governed by charge transfer and that inhibition efficiency increases with inhibitor adsorption. UV\u2013vis analysis suggested that the functional groups of DEAI form a complex with iron cations on the carbon steel surface. Surface characterization confirms the formation of a protective interfacial film. Atomic force microscopy (AFM) shows a significant reduction in surface roughness, while X-ray photoelectron spectroscopy (XPS) provides evidence of strong interactions between inhibitor molecules and the steel surface through Fe\u2013O and Fe\u2013N bonds. Ultraviolet photoelectron spectroscopy (UPS) reveals modifications in the electronic structure at the metal\u2013inhibitor interface, indicating enhanced surface passivation and strong electronic coupling. Adsorption follows a modified Langmuir isotherm and involves both physical and chemical interactions. Density functional theory and molecular dynamics simulations further support strong adsorption of DEAI on the Fe(110) surface. These findings provide comprehensive insight into the mechanism of inhibition and highlight the key role of interfacial interactions in corrosion protection.<\/jats:p>","DOI":"10.1021\/acsomega.6c06442","type":"journal-article","created":{"date-parts":[[2026,10,2]],"date-time":"2026-10-02T12:01:47Z","timestamp":1790942507000},"page":"61394-61418","source":"Crossref","is-referenced-by-count":0,"title":["Surface and Electrochemical\nInvestigation of a Novel\nIsoxazolone Inhibitor for Carbon Steel Corrosion: Adsorption and Inhibition\nMechanism"],"prefix":"10.1021","volume":"11","author":[{"given":"Chahrazed","family":"Rebie","sequence":"first","affiliation":[{"name":"University of Sai\u0308da , , ,","place":["Sai\u0308da, Algeria, 20000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Omar","family":"Benali","sequence":"additional","affiliation":[{"name":"University of Sai\u0308da , , ,","place":["Sai\u0308da, Algeria, 20000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Abdelghani","family":"Sehmi","sequence":"additional","affiliation":[{"name":"Higher Normal School of Sai\u0308da , , BP 138 , ,","place":["Sai\u0308da, Algeria, 20000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"M\u2019hamed","family":"Guezzoul","sequence":"additional","affiliation":[{"name":"National Polytechnic School (ENP) of Oran , , BP 1523 El-Mnaouar , ,","place":["Oran, Algeria, 31000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Farouk","family":"Boudou","sequence":"additional","affiliation":[{"name":"University of Science and Technology of Oran \u2212 Mohamed-Boudiaf (USTO-MB) , , ,","place":["Oran, Algeria, 31000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6698-0844","authenticated-orcid":true,"given":"Farouk","family":"Zaoui","sequence":"additional","affiliation":[{"name":"National Polytechnic School (ENP) of Oran , , BP 1523 El-Mnaouar , ,","place":["Oran, Algeria, 31000"]},{"name":"Universite\u0301 de Ain Te\u0301mouchent - Belhadj Bouchaib , , B.P 284 , ,","place":["Ain Te\u0301mouchent, Algeria, 46000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6752-3357","authenticated-orcid":true,"given":"Chakib","family":"Alaoui","sequence":"additional","affiliation":[{"name":"University of Science and Technology of Oran Mohamed Boudiaf , , M\u2019naouar, BP 1505 El , ,","place":["Oran, Algeria, 31000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-9915-0022","authenticated-orcid":true,"given":"Chems Eddine","family":"Gherdaoui","sequence":"additional","affiliation":[{"name":"Univ. Lille, CNRS, INRAE, Centrale Lille, UMR 8207 - UMET - Unite\u0301 Mate\u0301riaux et Transformations , ,","place":["Lille, France, F-59000"]},{"name":"Zone Industrielle ZAC Artoipole , , 170 Alle\u0301e de France, BP 22004 , ,","place":["Arras, France, 62060"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8722-9937","authenticated-orcid":true,"given":"Imadeddine","family":"Azzouz","sequence":"additional","affiliation":[{"name":"Sultan Qaboos University , , Al Khoudh, P.O. 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